1.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 2 h / 20 °C 1.3: pH 2 2.1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C View Scheme
参考文献
Spicer, Julie A.; Huttunen, Kristiina M.; Miller, Christian K.; Denny, William A.; Ciccone, Annette; Browne, Kylie A.; Trapani, Joseph A.
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 3 p. 1319 - 1336
1: With 1,1'-carbonyldiimidazole in tetrahydrofuran
T=20°C; 2 h;
2: With sodium tetrahydroborate in tetrahydrofuran; water
3: With hydrogenchloride in tetrahydrofuran; water
pH=2;
参考文献
PETER MACCALLUM CANCER INSTITUTE; SPICER, Julie Ann; HUTTUNEN, Kristiina Maria; LYONS, Dani Michelle; TRAPANI, Joseph Albert; SMYTH, Mark John; DENNY, William Alexander
Patent: WO2011/75784 A1, 2011 ;
Location in patent: Page/Page column 92-93 ;
