6H-苯并呋喃并[3,2-c][1]苯并吡喃-6-酮合成路线 （共 54 条）
反应条件
1: 50 percent / 85percent hydrazine hydrate / propan-1-ol / 60 h / Heating
2: 17 percent / yellow HgO / xylene / 2 h / Heating
4: 90 percent / PhMe3Si, I2 / 3 h / 110 °C
View Scheme
参考文献
Larock, Richard C.; Harrison, L. Wayne
Journal of the American Chemical Society, 1984 , vol. 106, # 15 p. 4218 - 4227
反应条件
1: 64 percent / CuSO4*5H2O / pyridine; H2O / 2 h / Heating
2: 50 percent / 85percent hydrazine hydrate / propan-1-ol / 60 h / Heating
3: 17 percent / yellow HgO / xylene / 2 h / Heating
5: 90 percent / PhMe3Si, I2 / 3 h / 110 °C
View Scheme
参考文献
Larock, Richard C.; Harrison, L. Wayne
Journal of the American Chemical Society, 1984 , vol. 106, # 15 p. 4218 - 4227
反应条件
1: 17 percent / yellow HgO / xylene / 2 h / Heating
3: 90 percent / PhMe3Si, I2 / 3 h / 110 °C
View Scheme
参考文献
Larock, Richard C.; Harrison, L. Wayne
Journal of the American Chemical Society, 1984 , vol. 106, # 15 p. 4218 - 4227
反应条件
1: 42 percent / KCN / ethanol; H2O / 4 h / Heating
2: 64 percent / CuSO4*5H2O / pyridine; H2O / 2 h / Heating
3: 50 percent / 85percent hydrazine hydrate / propan-1-ol / 60 h / Heating
4: 17 percent / yellow HgO / xylene / 2 h / Heating
6: 90 percent / PhMe3Si, I2 / 3 h / 110 °C
View Scheme
参考文献
Larock, Richard C.; Harrison, L. Wayne
Journal of the American Chemical Society, 1984 , vol. 106, # 15 p. 4218 - 4227
反应条件
1: 96 percent / CuI; PdCl2(PPh3)2; Et3N / dimethylformamide / 2 h / 60 °C
2: 95 percent / I2 / CH2Cl2 / 12 h / 25 °C
3: 99 percent / PdCl2(PPh3)2; K2CO3 / dimethylformamide / 6 h / 60 °C
View Scheme
参考文献
Yao, Tuanli; Yue, Dawei; Larock, Richard C.
Journal of Organic Chemistry, 2005 , vol. 70, # 24 p. 9985 - 9989
反应条件
1: 91 percent / dimethylformamide / 0.17 h / Heating
2: 95 percent / NEt3 / PdCl2 / 8 h / Heating
View Scheme
参考文献
Laschober; Kappe
Synthesis, 1990 , # 5 p. 387 - 388
反应条件
anhydrous iron chloride; silica gel in 1,2-dichloro-ethane
24 h; Reflux;
参考文献
Tang, Lina; Pang, Yongle; Yan, Qiao; Shi, Liuqing; Huang, Jianhui; Du, Yunfei; Zhao, Kang
Journal of Organic Chemistry, 2011 , vol. 76, # 8 p. 2744 - 2752
反应条件
palladium on activated charcoal in diphenylether
2 h; Heating;
参考文献
Majumdar, K C; Khan, A T; Gupta, A K; Kundu, A K; Choudhury, P K
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 10 p. 667 - 672
反应条件
1: 50 percent / Ag2CO3/Celite / acetonitrile / Heating
2: 79 percent / Pd/C / 3 h / 200 °C
View Scheme
参考文献
Lee, Yong Rok; Suk, Jung Yup; Kim, Byung So
Organic Letters, 2000 , vol. 2, # 10 p. 1387 - 1389
反应条件
1: pyridine / 1 h / 20 °C
2: 0.45 g / CuI; Et3N / PdCl2(PPh3)2 / dimethylformamide / 16 h / 60 °C
3: 90 percent / aq. NaOH / methanol / 0.5 h / 20 °C
4: 35 percent / CuCl2; NaOAc; K2CO3 / PdCl2 / acetonitrile / 20 h / 20 °C
View Scheme
参考文献
Hiroya, Kou; Suzuki, Naoyuki; Yasuhara, Akito; Egawa, Yuya; Kasano, Atsushi; Sakamoto, Takao
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 24 p. 4339 - 4346
