6H-苯并呋喃并[3,2-c][1]苯并吡喃-6-酮合成路线 （共 54 条）
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in benzene
36 h; Heating;
参考文献
Singh, Rishi Pal; Singh, Daljeet
Heterocycles, 1985 , vol. 23, # 4 p. 903 - 907
反应条件
1: With boron tribromide in dichloromethane
T=-78 - 20°C; Inert atmosphere;
2: With triethylamine in toluene
1 h; RefluxInert atmosphere;
3: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in toluene
24 h; RefluxInert atmosphere;
参考文献
Tricotet, Thomas; Fleming, Patricia; Cotter, Juliet; Hogan, Anne-Marie L.; Strohmann, Carsten; et al.
Journal of the American Chemical Society, 2009 , vol. 131, p. 3142 - 3143
反应条件
trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); potassium carbonate in 1,4-dioxane
T=140°C; 24 h; Schlenk technique; KineticsMechanism; Reagent/catalystSolventTemperature;
参考文献
Kapdi, Anant R.; Karbelkar, Amruta; Naik, Minal; Pednekar, Suhas; Fischer, Christian; Schulzke, Carola; Tromp, Moniek
RSC Advances, 2013 , vol. 3, # 43 p. 20905 - 20912
反应条件
phenyltrimethyl silane; iodine
T=110°C; 3 h;
参考文献
Larock, Richard C.; Harrison, L. Wayne
Journal of the American Chemical Society, 1984 , vol. 106, # 15 p. 4218 - 4227
反应条件
silica gel; pyridinium chlorochromate in dichloromethane
T=40°C; 4 h;
参考文献
Takeda, Norihiko; Miyata, Okiko; Naito, Takeaki
European Journal of Organic Chemistry, 2007 , # 9 p. 1491 - 1509
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in N,N-dimethyl-formamide
T=60°C; 6 h;
参考文献
Yao, Tuanli; Yue, Dawei; Larock, Richard C.
Journal of Organic Chemistry, 2005 , vol. 70, # 24 p. 9985 - 9989
反应条件
sodium acetate; potassium carbonate; copper dichloride; palladium dichloride in acetonitrile
T=20°C; 20 h;
参考文献
Hiroya, Kou; Suzuki, Naoyuki; Yasuhara, Akito; Egawa, Yuya; Kasano, Atsushi; Sakamoto, Takao
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 24 p. 4339 - 4346
反应条件
1: 80 percent / anhydrous potassium carbonate / acetone / 30 h / Heating
2: 69 percent / polyphosphoric acid / 2 h
3: 89 percent / 2,3-dichloro-5,6-dicyano-p-benzoquinone (DDQ) / benzene / 36 h / Heating
View Scheme
参考文献
Singh, Rishi Pal; Singh, Daljeet
Heterocycles, 1985 , vol. 23, # 4 p. 903 - 907
反应条件
triethylamine; palladium dichloride
8 h; Heating;
参考文献
Laschober; Kappe
Synthesis, 1990 , # 5 p. 387 - 388
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in benzene
72 h; Heating;
参考文献
Mali, R. S.; Tilve, S. G.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, # 1-12 p. 465
