sodium hydroxide in methanol 8 h; Heating;

1: LiAlH4 View Scheme

1: LiAlH4 View Scheme

1: LiAlH4 View Scheme

暂无反应条件数据

1.1: 90 percent / aq. NaOH / methanol / 8 h / Heating 2.1: 85 percent / CBr4; PPh3; pyridine / CH2Cl2 3.1: tetrahydrofuran / 0.33 h / -20 °C 4.1: n-BuLi; t-BuOH / tetrahydrofuran; hexane / 0.33 h / -78 °C 4.2: 8 percent / tetrahydrofuran; hexane / 3 h 5.1: NaBH4 / methanol / 0.33 h / 0 °C 6.1: 254.8 mg / Et3N; DMAP / CH2Cl2 / 5 h / 25 °C 7.1: aq. CAN / acetonitrile / 0.25 h / 25 °C 7.2: aq. NaOH / 1 h / 25 °C View Scheme

ammonium acetate; acetic acid in benzene 40 h; Heating;

in N,N-dimethyl-formamide T=25°C; 48 h;

sodium cyanide in N,N-dimethyl-formamide T=50°C; 2 h;

in N,N-dimethyl-formamide T=0 - 30°C;