diisobutylaluminium hydride in toluene
T=-78°C; 0.25 h;
参考文献
Doi, Fuminao; Ohara, Taiga; Ogamino, Takahisa; Higashinakasu, Keiko; Hasegawa, Koji; Nishiyama, Shigeru
Bulletin of the Chemical Society of Japan, 2004 , vol. 77, # 12 p. 2257 - 2263
1: bromine / CHCl3 / 2.5 h / 20 °C
2: K2CO3 / dimethylformamide / 21 h / 20 °C
3: 26.5 g / dimethylformamide / 26 h / 130 °C
4: 82 percent / DIBAL-H / toluene / 0.25 h / -78 °C
View Scheme
参考文献
Doi, Fuminao; Ohara, Taiga; Ogamino, Takahisa; Higashinakasu, Keiko; Hasegawa, Koji; Nishiyama, Shigeru
Bulletin of the Chemical Society of Japan, 2004 , vol. 77, # 12 p. 2257 - 2263
1: K2CO3 / dimethylformamide / 21 h / 20 °C
2: 26.5 g / dimethylformamide / 26 h / 130 °C
3: 82 percent / DIBAL-H / toluene / 0.25 h / -78 °C
View Scheme
参考文献
Doi, Fuminao; Ohara, Taiga; Ogamino, Takahisa; Higashinakasu, Keiko; Hasegawa, Koji; Nishiyama, Shigeru
Bulletin of the Chemical Society of Japan, 2004 , vol. 77, # 12 p. 2257 - 2263
