2-(4-甲基苯基)-1-异吲哚啉酮合成路线 (共 10 条)
反应条件
bis(benzonitrile)palladium(II) dichloride; triphenylphosphine in N,N-dimethyl-formamide
T=100°C; P=7600.51 Torr; 24 h; Autoclave;
参考文献
Cho, Chan Sik; Ren, Wen Xiu
Tetrahedron Letters, 2009 , vol. 50, # 18 p. 2097 - 2099
反应条件
Co-phthalocyanine; (Ph)2SiH2 in ethanol
T=20 - 70°C; 5 h; Green chemistry; chemoselective reaction;
参考文献
Kumar, Vishal; Sharma, Upendra; Singh, Bikram; Kumar, Neeraj
Australian Journal of Chemistry, 2012 , vol. 65, # 12 p. 1594 - 1598
反应条件
bi(8F-5acetoxy-5H-10oxa-4b-aza-5Pd-indeno[2,1-a]inden-5-yl); potassium carbonate in N,N-dimethyl-formamide
T=80°C; P=760 Torr; 12 h;
参考文献
Grigg, Ronald; Zhang, Lixin; Collard, Simon; Keep, Ann
Tetrahedron Letters, 2003 , vol. 44, # 37 p. 6979 - 6982
反应条件
1: 2-(fluoromethyl)bromobenzene With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.5 h; Inert atmosphere;
2: 4-methyl phenyl isocyanate in tetrahydrofuran; hexane
T=-78 - 20°C; 16 h; Inert atmosphere;
参考文献
Zhang, Laijun; Zhang, Wei; Liu, Jun; Hu, Jinbo
Journal of Organic Chemistry, 2009 , vol. 74, # 7 p. 2850 - 2853
反应条件
tert-butyl benzene; hydrogen; platinum in 1,4-dioxane
T=80°C; P=750.075 Torr; Sealed tube;
参考文献
Shi, Linyan; Hu, Lei; Wang, Jiaqing; Cao, Xueqin; Gu, Hongwei
Organic Letters, 2012 , vol. 14, # 7 p. 1876 - 1879
反应条件
1,2,3-Benzotriazole; borate buffer; 2-hydroxyethanethiol in acetonitrile
13 h; Ambient temperature;
参考文献
Takahashi, Ichiro; Hatanaka, Minoru
Heterocycles, 1997 , vol. 45, # 12 p. 2475 - 2499
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; potassium carbonate in N,N-dimethyl acetamide
T=120°C; 2 h; Inert atmosphere;
参考文献
Zheng, Yu; Yu, Gongli; Wu, Jinlong; Dai, Wei-Min
Synlett, 2010 , # 7 p. 1075 - 1080
反应条件
hydrogenchloride; methanol; tin
参考文献
Borsche et al.
Chemische Berichte, 1934 , vol. 67, p. 675,681
反应条件
T=100°C; Behandeln des erhaltenen Reaktionsgemisches mit wss. Natriumcarbonat-Loesung unter Einleiten von Wasserdampf;
参考文献
Borsche et al.
Chemische Berichte, 1934 , vol. 67, p. 675,681
反应条件
pyridine; diphosphorus pentasulfide
T=140 - 150°C;
参考文献
Kovtunenko, V. A.; Dobrenko, T. T.; Voitenko, Z. V.; Tyltin, A. K.; Babichev, F. S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1984 , vol. 20, # 9 p. 978 - 983
Khimiya Geterotsiklicheskikh Soedinenii, 1984 , vol. 20, # 9 p. 1200 - 1205