1,4-环己二烯-1,2-二羧基酸酐合成路线 （共 13 条）
参考文献
Flaig
Justus Liebigs Annalen der Chemie, 1950 , vol. 568, p. 1,28
反应条件
1: Ph2C=O / Irradiation
2: LiAlH4
3: p-TsOH
4: Na/NH3
5: 60percent aq. AcOH
6: pyridine
7: 1.) MeSCH2S(O)Me, 2.) BuLi, 3.) H2SO4
8: C5H5NHBr3, pyridine / CH2Cl2
9: LiCl, Li2CO3, HMPA
10: EtONa / benzene
11: p-TsN3, triethylamine / diethyl ether
12: Irradiation
13: 100 percent / 5percent aq. NaOH / methanol / 6 h / 12 °C
14: triethylamine, (PhO)2P(O)N3 / benzene / 20 h / Heating
15: 18 h / Heating
16: 1.) NaHCO3, Me2SO4, 2.) NaOH / 1.) MeOH, 35 deg C, 40 h, 2.) MeOH, H2O, 40 deg C, 2 h
View Scheme
参考文献
Tsuji, Takashi; Nishida, Shinya; Okuyama, Masahiro; Osawa, Eiji
Journal of the American Chemical Society, 1995 , vol. 117, # 39 p. 9804 - 9813
参考文献
Kucherov,V.F.; Grigor'eva,N.Ya.
J. Gen. Chem. USSR (Engl. Transl.), 1961 , vol. 31, # 2 p. 447 - 457,408 - 415
