N-(3-氨基丙基)苯二甲酰亚胺合成路线 （共 6 条）
反应条件
hydrogenchloride; hydrogen; platinum(IV) oxide in ethanol
P=760 Torr;
参考文献
Prabhakaran; Woo; Yorgey; Gould
Journal of the American Chemical Society, 1988 , vol. 110, # 17 p. 5785 - 5791
反应条件
1: 84 percent / dimethylsulfoxide / 6 h / 65 °C
2: H2, conc. HCl / PtO2 / ethanol / 760 Torr
View Scheme
参考文献
Prabhakaran; Woo; Yorgey; Gould
Journal of the American Chemical Society, 1988 , vol. 110, # 17 p. 5785 - 5791
反应条件
sodium hypophosphite monohydrate; 5 palladium on charcoal; hypophosphorous acid in 2-methyl tetrahydrofuran; water
7 h; Sonication; chemoselective reaction;
参考文献
Baron, Marc; Metay, Estelle; Lemaire, Marc; Popowycz, Florence
Green Chemistry, 2013 , vol. 15, # 4 p. 1006 - 1015
反应条件
2: palladium; methanol / Hydrogenation
View Scheme
参考文献
v. Braun; Pinkernelle
Chemische Berichte, 1934 , vol. 67, p. 1056,1220
参考文献
Daublain, Pierre; Thazhathveetil, Arun K.; Shafirovich, Vladimir; Wang, Qiang; Trifonov, Anton; Fiebig, Torsten; Lewis, Frederick D.
Journal of Physical Chemistry B, 2010 , vol. 114, # 45 p. 14265 - 14272
反应条件
1: Et3N / CH2Cl2 / 24 h / Ambient temperature
2: 87 percent / Ac2O, sodium nitrite / acetic acid / 10 h / 0 °C
3: 0.78 g / Na2CO3 / CCl4 / 24 h / Heating
4: NaI / acetone / 20 h / Heating
View Scheme
参考文献
Prabhakaran; Woo; Yorgey; Gould
Journal of the American Chemical Society, 1988 , vol. 110, # 17 p. 5785 - 5791
