反应条件
1: 93 percent / 2,6-lutidine / CH2Cl2 / 4 h / 0 °C 2: 1.) lithium hexamethyldisilazide, 2.) acetic acid / 1.) THF, 0 deg C, 40 min, 2.) THF, -78 deg C, 10 min 3: 79 percent / triethylammonium fluoride / acetonitrile / 72 h / Ambient temperature View Scheme
参考文献
Andrews, Robert C.; Teague, Simon J.; Meyers, A. I.
Journal of the American Chemical Society, 1988 , vol. 110, # 23 p. 7854 - 7858
