N-甲基-1,2-苯二胺合成路线 （共 142 条）
参考文献
CIBA
Patent: US2828317 , 1955 ;
反应条件
(i) (heating), (ii) sulfur, benzene; Multistep reaction;
参考文献
Anisimova,O.S. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1976 , vol. 46, p. 808 - 813,807 - 811
参考文献
Dannley,R.L.; Grava,A.
Canadian Journal of Chemistry, 1965 , vol. 43, p. 3377 - 3386
反应条件
in various solvent(s)
T=170 - 190°C; Condensation;
参考文献
Elgafi, Sarah; Field, Leslie D.; Messerle, Barbara A.; Turner, Peter; Hambley, Trevor W.
Journal of Organometallic Chemistry, 1999 , vol. 588, # 1 p. 69 - 77
参考文献
McKinnon, David M.; Spevack, Perry; Tipples, Graham
Canadian Journal of Chemistry, 1988 , vol. 66, p. 2339 - 2344
反应条件
1: 71 percent / Et3N / CH2Cl2 / 20 °C
2: 83 percent / phosphorous oxychloride; Huning's base / toluene / 110 °C
View Scheme
参考文献
Cheeseman
Journal of the Chemical Society, 1955 , p. 1804,1806
反应条件
1: 36 percent / pyridine / tetrahydrofuran / 1 h / Ambient temperature
2: 70 percent / benzene / 0.17 h / 80 °C
View Scheme
参考文献
Rakitin, Oleg A.; Rees, Charles W.; Vlasova, Olga G.
Tetrahedron Letters, 1996 , vol. 37, # 26 p. 4589 - 4592
参考文献
Konstantinova, Lidia S.; Rakitin, Oleg A.; Rees, Charles W.; Sivadasan, Sivaprasad; Torroba, Tomas
Tetrahedron, 1998 , vol. 54, # 33 p. 9639 - 9650
反应条件
in 1,4-dioxane
Heating;
参考文献
Huang, Zhi-Tang; Wang, Mei-Xiang
Tetrahedron, 1992 , vol. 48, # 12 p. 2325 - 2332
反应条件
2: dimethyl sulfate; aqueous KOH
View Scheme
参考文献
Cheeseman
Journal of the Chemical Society, 1955 , p. 1804,1806
