N-甲基-1,2-苯二胺合成路线 （共 142 条）
反应条件
hydrogen; palladium on activated charcoal in methanol T=20°C; 0.5 h;
参考文献
Li, Qun; Li, Tongmei; Woods, Keith W.; Gu, Wen-Zhen; Cohen, Jerry; Stoll, Vincent S.; Galicia, Tomas; Hutchins, Charles; Frost, David; Rosenberg, Saul H.; Sham, Hing L.
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 11 p. 2918 - 2922
反应条件
sodium hydroxide; CaCl2 in diethyl ether; ethanol
参考文献
The State of Oregon, acting by and through The Oregon State Board of Higher Education, acting for and on behalf of The Oregon Health Sciences University; The University of Oregon; The Regents of the University of California
Patent: US5514680 A1, 1996 ;
US 5514680 A
反应条件
tetreamethyl ammonium hydroxide in methanol; ethanol; benzene
参考文献
Texaco Development Corporation
Patent: US4169853 A1, 1979 ;
反应条件
lead (II) nitrate T=169.85°C; 0.5 h;
参考文献
Fu, Yue; Baba, Toshihide; Ono, Yoshio
Journal of Catalysis, 2001 , vol. 197, # 1 p. 91 - 97
反应条件
sodium amide; 1,8-diamino-naphthalene in xylene T=120 - 130°C; 3 h;
参考文献
Konstantinchenko, A. A.; Pozharskii, A. F.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 7.2 p. 1191 - 1194
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 7 p. 1432 - 1436
反应条件
zeolite NaY 2 h; Heating;
参考文献
Ebenezer, Warren J.; Hutchings, Michael G.; Jones, Ken; Lambert, David A.; Watt, Ian
Tetrahedron Letters, 2007 , vol. 48, # 9 p. 1641 - 1643
反应条件
1: 82 percent / Et3N / CH2Cl2 / Ambient temperature 2: 86 percent / K2CO3 / dimethylformamide / 0.25 h / 60 - 70 °C 3: 59 percent / cyclohexene / 10percent Pd/C / ethanol / Heating 4: 7percent aq. Na2CO3 / Heating View Scheme
参考文献
Mack, Robert A.; Georgiev, Vassil St.; Wu, Edwin S. C.; Matz, James R.
Journal of Organic Chemistry, 1993 , vol. 58, # 22 p. 6158 - 6162
反应条件
1: 86 percent / K2CO3 / dimethylformamide / 0.25 h / 60 - 70 °C 2: 59 percent / cyclohexene / 10percent Pd/C / ethanol / Heating 3: 7percent aq. Na2CO3 / Heating View Scheme
参考文献
Mack, Robert A.; Georgiev, Vassil St.; Wu, Edwin S. C.; Matz, James R.
Journal of Organic Chemistry, 1993 , vol. 58, # 22 p. 6158 - 6162
反应条件
1: 59 percent / cyclohexene / 10percent Pd/C / ethanol / Heating 2: 7percent aq. Na2CO3 / Heating View Scheme
参考文献
Mack, Robert A.; Georgiev, Vassil St.; Wu, Edwin S. C.; Matz, James R.
Journal of Organic Chemistry, 1993 , vol. 58, # 22 p. 6158 - 6162
反应条件
1: 35 percent / H2 / 10percent Pd/C / ethanol 2: 25 percent / NH2OH*HCl, NaOAc / ethanol; H2O / Ambient temperature View Scheme
参考文献
Essassi, El Mokhtar; Salem, Moussa; Viallefont, Philippe
Bulletin de la Societe Chimique de France, 1987 , # 5 p. 890 - 892
