1-BOC-5-甲基吲哚-2-硼酸合成路线 （共 3 条）
反应条件
1: With tri-isopropoxy-borane; lithium diisopropyl amide in tetrahydrofuran T=0°C; 3 h; 2: in tetrahydrofuran pH=6; aq. phosphate buffer;
参考文献
Kanamori, Takashi; Masaki, Yoshiaki; Mizuta, Masahiro; Tsunoda, Hirosuke; Ohkubo, Akihiro; Sekine, Mitsuo; Seio, Kohji
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 5 p. 1007 - 1013
反应条件
1.1: DMAP / CH2Cl2 / 0.75 h / 20 °C 2.1: (iPrO)3B; LDA / tetrahydrofuran / 0.5 h / 0 - 5 °C 2.2: 85 percent / 2N HCl / tetrahydrofuran View Scheme
参考文献
Kanamori, Takashi; Masaki, Yoshiaki; Mizuta, Masahiro; Tsunoda, Hirosuke; Ohkubo, Akihiro; Sekine, Mitsuo; Seio, Kohji
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 5 p. 1007 - 1013
反应条件
1.1: DMAP / CH2Cl2 / 0.75 h / 20 °C 2.1: (iPrO)3B; LDA / tetrahydrofuran / 0.5 h / 0 - 5 °C 2.2: 85 percent / 2N HCl / tetrahydrofuran View Scheme
参考文献
Kanamori, Takashi; Masaki, Yoshiaki; Mizuta, Masahiro; Tsunoda, Hirosuke; Ohkubo, Akihiro; Sekine, Mitsuo; Seio, Kohji
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 5 p. 1007 - 1013
