6-甲基环己-1,3-二烯-1-甲醛合成路线 （共 21 条）
参考文献
Grundmann
Chemische Berichte, 1948 , vol. 81, p. 512
参考文献
Grundmann; Loew
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1938 , vol. 256, p. 141,151
反应条件
piperidine; acetic acid
0.25 h; Heating; Yields of byproduct given;
参考文献
D'Amico, Kevin L.; Manos, Christopher; Christensen, Ronald L.
Journal of the American Chemical Society, 1980 , vol. 102, # 6 p. 1777 - 1782
反应条件
sodium hydroxide; tetra-(n-butyl)ammonium iodide in dichloromethane
1) 2.5 h, 0 deg C 2) 20 min, reflux; other catalysts, other normality of NaOH;
参考文献
McIntosh, John M.; Khalil, Hamdy; Pillon, David W.
Journal of Organic Chemistry, 1980 , vol. 45, # 17 p. 3436 - 3439
反应条件
sodium hydroxide; N-hexadecyl-N,N,N-trimethylammonium bromide in dichloromethane
参考文献
McIntosh, John M.; Khalil, Hamdy; Pillon, David W.
Journal of Organic Chemistry, 1980 , vol. 45, # 17 p. 3436 - 3439
反应条件
sodium acetate
T=150°C; 10 h; Yield given. Yields of byproduct given;
参考文献
Banks, Robert E.; Miller, Allen J.; Nunn, John M.; Stanley, Philip; Weakley, Timothy J. R.; Ullah, Zakir
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1096 - 1102
反应条件
hydrogenchloride; hydroquinone
1) 130 deg C, 7 h, sealed tube; 2) 95-100 deg C, 1 h.; Yield given. Multistep reaction;
参考文献
Makin, S. M.; Tung, Nguyen Fyong; Shavrygina, O. A.; Arshava, B. M.; Romanova, I. A.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 4 p. 640 - 645
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 4 p. 727 - 732
反应条件
N,N,N',N,-tetramethylethylenediamine; lithium diisopropyl amide
THF; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Moorhoff, Cornelis M.; Schneider, David F.
Tetrahedron Letters, 1987 , vol. 28, # 40 p. 4721 - 4724
反应条件
hydrogenchloride; hydroquinone; dihydroquinine
1) 150 deg C, 7 h, sealed tube, 2) reflux, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Makin, S. M.; Shavrygina, O. A.; Nguyen, Fong Tung
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 11 p. 2082 - 2087
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 11 p. 2309 - 2315
反应条件
N,N,N',N,-tetramethylethylenediamine; lithium diisopropyl amide
THF; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Moorhoff, Cornelis M.; Schneider, David F.
Tetrahedron Letters, 1987 , vol. 28, # 40 p. 4721 - 4724
