N,N'-双(2-氨乙基)-1,3-丙二胺合成路线 （共 19 条）
参考文献
Mashuta, Mark S.; Pimenov, Konstantin V.; Grapperhaus, Craig A.
Acta Crystallographica Section C: Crystal Structure Communications, 2002 , vol. 58, # 4 p. o226-o227
反应条件
Yield given. Multistep reaction;
参考文献
Mochizuki, Katsura; Gotoh, Hajime; Suwabe, Masaaki; Sakakibara, Tohru
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 6 p. 1750 - 1756
反应条件
1: acetonitrile; H2O / 4 h / 4 °C 2: K2CO3 / acetonitrile; H2O / Heating 3: 51 percent / acetonitrile / 20 °C 4: 82 percent / aq. NaOH / 20 °C View Scheme
参考文献
Boschetti, Frederic; Denat, Franck; Espinosa, Enrique; Guilard, Roger
Chemical Communications, 2002 , # 4 p. 312 - 313
反应条件
in ethanol 168 h; Heating;
参考文献
Fabbrizzi, Luigi; Licchelli, Maurizio; Pallavicini, Piersandro; Perotti, Angelo; Taglietti, Angelo; Sacchi, Donata
Chemistry--A European Journal, 1996 , vol. 2, # 1 p. 75 - 82
反应条件
in ethanol 3 h; Heating;
参考文献
Kimura, Eiichi; Shionoya, Mitsuhiko; Okamoto, Miho; Nada, Hiroko
Journal of the American Chemical Society, 1988 , vol. 110, p. 3679 - 3680
反应条件
in methanol
384 h; Heating;
参考文献
Kimura,Eiichi; Koike, Tohru; Nada, Hiroko; Iitaka, Yoichi
Journal of the Chemical Society, Chemical Communications, 1986 , # 17 p. 1322 - 1323
反应条件
1: 74.6 percent / aq. NaOH / diethyl ether / 1 h / Ambient temperature
2: 78.3 percent / K2CO3 / dimethylformamide / 8 h / 110 °C
3: 35 percent / 96percent aq. H2SO4 / 50 h / 110 °C
4: 1.2 g / dimethylformamide / 2 h / 110 - 120 °C
View Scheme
参考文献
Meunier, I.; Mishra, A. K.; Hanquet, B.; Cocolios, P.; Guilard, R.
Canadian Journal of Chemistry, 1995 , vol. 73, # 5 p. 685 - 695
反应条件
1: 74.6 percent / aq. NaOH / diethyl ether / 1 h / Ambient temperature
2: 78.3 percent / K2CO3 / dimethylformamide / 8 h / 110 °C
View Scheme
参考文献
Pisareva, S. A.; Bel'skii, F. I.; Medved', T. Ya.; Kabachnik, M. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 2 p. 372 - 376
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 2 p. 413 - 417
反应条件
in water
T=0 - 20°C; 11 h;
参考文献
Centre National de la Recherche Scientifique (C.N.R.S.); Commissariat a l'energie Atomique
Patent: US7312327 B2, 2007 ;
Location in patent: Page/Page column 12 ;
