6-甲氧基-3H-异苯并呋喃-1-酮合成路线 （共 34 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 3 h; Heating;
参考文献
Bhattacharjee, Debkumar; Popp, Frank D.
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 315 - 320
参考文献
Ikeda et al.
Kanazawa Daigaku Yakugakubu Kenkyu Nempo, 1957 , vol. 7, p. 64
Chem.Abstr., 1958 , p. 9025
反应条件
permanganate(VII) ion
参考文献
Journal of the Chemical Society, , p. 199
反应条件
potassium permanganate; hydroxide
参考文献
Leblois, Danielle; Piessard, Sylvie; Baut, Guillaume Le; Kumar, Piyush; Brion, Jean-Daniel; et al.
European Journal of Medicinal Chemistry, 1987 , vol. 22, p. 229 - 238
反应条件
air; lithium diisopropyl amide 1.) THF, -70 - -60 deg C, 2.) THF, 20 deg C, 22 h; Yield given. Multistep reaction;
参考文献
Dodsworth, David J.; Calcagno, Maria-Pia; Ehrmann, E. Ursula; Devadas, Bhatt; Sammes, Peter G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2120 - 2124
反应条件
1: With hydrogenchloride; acetic acid in water
T=20 - 90°C;
2: With morpholine in toluene
T=80°C; 2 h;
3: With sulfuric acid in water; toluene
参考文献
Koeberle, Solveigh C.; Fischer, Stefan; Schollmeyer, Dieter; Schattel, Verena; Gruetter, Christian; Rauh, Daniel; Laufer, Stefan A.
Journal of Medicinal Chemistry, 2012 , vol. 55, # 12 p. 5868 - 5877
反应条件
dipotassium hydrogenphosphate; palladium diacetate
T=140°C; 36 h; Sealed tube;
参考文献
Teixeira; Pereira; Da Silva; Guilardi; Paixao; Anconi; De Almeida; Ellena; Forlani
Journal of Molecular Structure, 2014 , vol. 1061, # 1 p. 61 - 68
反应条件
hydrogenchloride; sodium hydroxide; formaldehyd in dichloromethane
参考文献
Zambon Group S.p.A.
Patent: US6525055 B1, 2003 ;
反应条件
hydrogenchloride; sodium hydroxide; formaldehyd in methanol; dichloromethane; water
参考文献
Zambon Group S.p.A.
Patent: US6329370 B1, 2001 ;
反应条件
hydrogenchloride in water
T=70 - 80°C;
参考文献
Singh, Anil K.; Khade, Prashant K.
Tetrahedron Letters, 2011 , vol. 52, # 38 p. 4899 - 4902
