1,4-苯并二氧六环-2-甲酸乙酯合成路线 （共 44 条）
参考文献
Koo et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 5373
参考文献
Journal of the American Chemical Society, , vol. 77, p. 5373
参考文献
Koo et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 5373
反应条件
1: 1.) AlCl3, 2.) 28percent NH4OH / 1.) CS2, 0 deg C, 2.) EtOH 2: 57 percent / HCl / Heating 3: 1.) MCPBA, 2.) 10 N KOH / 1.) CH2Cl2, reflux, 18 h 4: 1.) KOH, 2.) HCl 5: 80 percent / EDCl, DMAP / CH2Cl2 6: BBr3 / CH2Cl2 / Ambient temperature 7: 1.) APTS, 2.) Et3N / 1.) reflux 8: 1.) H2, 2.) LiAlH4 / 1.) Pd/C / 1.) MeOH, 2.) Et2O, reflux View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 5, # 4 p. 535 - 536
参考文献
Chou, Wen-Chih; Tan, Chang-Wei; Chen, Shyh-Fong; Ku, Hao
Journal of Organic Chemistry, 1998 , vol. 63, # 26 p. 10015 - 10017
参考文献
Organic Preparations and Procedures International, , vol. 35, # 6 p. 603 - 608
反应条件
1: 65 percent / 6 h / 70 - 80 °C 2: 83 percent / butan-1-ol / 5 h / Heating View Scheme
参考文献
Kumaraswamy; Das; Jena, Nivedita
Organic Preparations and Procedures International, 2003 , vol. 35, # 6 p. 603 - 608
反应条件
1: 65 percent / 6 h / 70 - 80 °C 2: butan-1-ol / 5 h / Heating View Scheme
参考文献
Kumaraswamy; Das; Jena, Nivedita
Organic Preparations and Procedures International, 2003 , vol. 35, # 6 p. 603 - 608
反应条件
1: in methanol; isopropyl alcohol Heating; 2: With hydrogenchloride pH=2;
参考文献
Ramesh, Chakka; Reddy, Reguri Buchi; Reddy, Ghanta Mahesh
Heterocyclic Communications, 2006 , vol. 12, # 5 p. 373 - 376
参考文献
Koo et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 5373
