联苯-4,4-草酸二乙酯合成路线 (共 84 条)
参考文献
Doebner
Justus Liebigs Annalen der Chemie, 1874 , vol. 172, p. 111
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Reflux; Cooling with ice 2: pyridinium chlorochromate / dichloromethane / 2 h / Molecular sieve; Inert atmosphere; Reflux View Scheme
参考文献
Gurung, Santosh K.; Kim, Soo Bae; Park, Haeil
Archives of Pharmacal Research, 2010 , vol. 33, # 12 p. 1919 - 1926
反应条件
lithium aluminium tetrahydride in tetrahydrofuran Inert atmosphereRefluxCooling with ice;
参考文献
Gurung, Santosh K.; Kim, Soo Bae; Park, Haeil
Archives of Pharmacal Research, 2010 , vol. 33, # 12 p. 1919 - 1926
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 8 h / 20 °C / Reflux 2: carbon tetrabromide; triphenylphosphine / dichloromethane / 0 - 20 °C View Scheme
参考文献
Conejo-Garcia, Ana; Pisani, Leonardo; Del Carmen Nunez, Maria; Catto, Marco; Nicolotti, Orazio; Leonetti, Francesco; Campos, Joaquin M.; Gallo, Miguel A.; Espinosa, Antonio; Carotti, Angelo
Journal of Medicinal Chemistry, 2011 , vol. 54, # 8 p. 2627 - 2645