2,6,6-三甲基-1-环己烯基乙醛合成路线 （共 26 条）
反应条件
in tetrachloromethane (i) AIBN, (irradiation), (ii) CF3CO2H; Multistep reaction;
参考文献
Mantione,R.; Normant,H.
Bulletin de la Societe Chimique de France, 1973 , p. 2261 - 2265
反应条件
(i), (ii) Ph3SiOH, (iii) (Ph3SiO)3VO; Multistep reaction;
参考文献
Branca,S.J. et al.
Journal of Organic Chemistry, 1977 , vol. 42, # 19 p. 3165 - 3168
反应条件
1: 52 percent / t-BuOK / tetrahydrofuran / 1 h / Heating 2: 100 percent / AsPh3 / Pd2dba3*CHCl3 / dimethylformamide / 2 h / 20 °C View Scheme
参考文献
Wada, Akimori; Ieki, Yasuhiro; Ito, Masayoshi
Synlett, 2002 , # 7 p. 1061 - 1064
反应条件
3-chloro-benzenecarboperoxoic acid in tetrachloromethane T=0 - 30°C; 3 h; Yields of byproduct given;
参考文献
Nickson, Thomas E.
Tetrahedron Letters, 1986 , vol. 27, # 13 p. 1433 - 1436
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform 17 h; Heating;
参考文献
Nickson, Thomas E.
Tetrahedron Letters, 1986 , vol. 27, # 13 p. 1433 - 1436
反应条件
sodium nitrate; potassium dihydrogenphosphate; D-glucose; cornsteep liquor; Lasiodiplodia theobromae ATCC 28570; potassium chloride in ethanol T=28°C; biotransformation;
参考文献
Krasnobajew, Victor; Helmlinger, Daniel
Helvetica Chimica Acta, 1982 , vol. 65, # 5 p. 1590 - 1601
反应条件
3-chloro-benzenecarboperoxoic acid in tetrachloromethane T=0 - 30°C; 3 h; Yields of byproduct given;
参考文献
Nickson, Thomas E.
Tetrahedron Letters, 1986 , vol. 27, # 13 p. 1433 - 1436
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform 17 h; Heating;
参考文献
Nickson, Thomas E.
Tetrahedron Letters, 1986 , vol. 27, # 13 p. 1433 - 1436
反应条件
sodium nitrate; potassium dihydrogenphosphate; D-glucose; cornsteep liquor; Lasiodiplodia theobromae ATCC 28570; potassium chloride in ethanol T=28°C; biotransformation;
参考文献
Krasnobajew, Victor; Helmlinger, Daniel
Helvetica Chimica Acta, 1982 , vol. 65, # 5 p. 1590 - 1601
反应条件
1: LiAlH4
2: hydroxylation
View Scheme
参考文献
Krasnobajew, Victor; Helmlinger, Daniel
Helvetica Chimica Acta, 1982 , vol. 65, # 5 p. 1590 - 1601
