1: 3M HCl / 2 h / 80 °C
2: 190 g / toluene / 3 h / 80 - 90 °C
3: Zn, KH2PO4 / tetrahydrofuran; H2O / 2 h / the temperature is kept below 30 deg C
4: NaBH4 / methanol / 1.5 h / Heating
View Scheme
参考文献
Lassen; Perregaard
1983 , vol. 37, # 4 B p. 335 - 340
1: AcOH, conc. HCl / 1.5 h / Heating
2: t-BuOK / toluene / 2 h / 85 °C
3: 3M HCl / 2 h / 80 °C
4: 190 g / toluene / 3 h / 80 - 90 °C
5: Zn, KH2PO4 / tetrahydrofuran; H2O / 2 h / the temperature is kept below 30 deg C
6: NaBH4 / methanol / 1.5 h / Heating
View Scheme
参考文献
Lassen; Perregaard
1983 , vol. 37, # 4 B p. 335 - 340
1: 190 g / toluene / 3 h / 80 - 90 °C
2: Zn, KH2PO4 / tetrahydrofuran; H2O / 2 h / the temperature is kept below 30 deg C
3: NaBH4 / methanol / 1.5 h / Heating
View Scheme
参考文献
Lassen; Perregaard
1983 , vol. 37, # 4 B p. 335 - 340
1: t-BuOK / toluene / 2 h / 85 °C
2: 3M HCl / 2 h / 80 °C
3: 190 g / toluene / 3 h / 80 - 90 °C
4: Zn, KH2PO4 / tetrahydrofuran; H2O / 2 h / the temperature is kept below 30 deg C
5: NaBH4 / methanol / 1.5 h / Heating
View Scheme
参考文献
Lassen; Perregaard
1983 , vol. 37, # 4 B p. 335 - 340
