4,4'-二甲氧基-3,3',5,5'-四甲基联苯合成路线 (共 4 条)
反应条件
triphenylphosphine; nickel dichloride; zinc in N,N-dimethyl-formamide
T=50 - 60°C; 12 h;
参考文献
Yamato, Takehiko; Hideshima, Chieko; Suehiro, Kazuaki; Tashiro, Masashi; Prakash, G. K. Surya; Olah, George A.
Journal of Organic Chemistry, 1991 , vol. 56, # 21 p. 6248 - 6250
反应条件
[MoCl5] in dichloromethane
T=0°C; 0.5 h;
参考文献
Mirk, Daniela; Wibbeling, Birgit; Froehlich, Roland; Waldvogel, Siegfried R.
Synlett, 2004 , # 11 p. 1970 - 1974
反应条件
tetra-n-butylammonium tetrafluoroborate in dichloromethane; trifluoroacetic acid
T=12°C; electrolysis, other solvent; Further byproducts given;
参考文献
Ronlan, Alvin; Aalstad, Bjoerg; Parker, Vernon D.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1982 , vol. 36, # 5 p. 317 - 326
参考文献
Rathore; Bosch; Kochi
Tetrahedron, 1994 , vol. 50, # 23 p. 6727 - 6758