3,4-二氢-2,2-二甲基-2H-萘并[1,2-B]吡喃-5,6-二酮合成路线 (共 56 条)
反应条件
sulfuric acid T=20°C; 0.25 h;
参考文献
Bian, Jinlei; Deng, Bang; Zhang, Xiaojin; Hu, Tianhan; Wang, Nan; Wang, Wei; Pei, Haixiang; Xu, Yu; Chu, Hongxi; Li, Xiang; Sun, Haopeng; You, Qidong
Tetrahedron Letters, 2014 , vol. 55, # 8 p. 1475 - 1478
反应条件
sulfuric acid in water 3 h;
参考文献
Paterno
Gazzetta Chimica Italiana, 1882 , vol. 12, p. 353
反应条件
sulfuric acid in acetic acid T=20°C; 0.333333 h;
参考文献
Claessens, Sven; Habonimana, Pascal; De Kimpe, Norbert
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 16 p. 3790 - 3795
反应条件
ammonium cerium(IV) nitrate; water in acetonitrile T=0 - 5°C; Oxidation; 0.5 h;
参考文献
Alves, Glaucia B. C.; Lopes, Rosangela S. C.; Lopes, Claudio C.; Snieckus, Victor
Synthesis, 1999 , # 11 p. 1875 - 1877
反应条件
nitric acid in acetic acid T=10°C; Oxidation; 2 h;
参考文献
Alves, Glaucia B. C.; Lopes, Rosangela S. C.; Lopes, Claudio C.; Snieckus, Victor
Synthesis, 1999 , # 11 p. 1875 - 1877
反应条件
nitric acid in acetic acid T=0°C; 2 h;
参考文献
Amaral; Barnes
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 6 p. 1457 - 1460
反应条件
1: in 1,4-dioxane Knoevenagel condensation; Reflux; 2: With sulfuric acid in 1,4-dioxane T=20°C; 0.5 h;
参考文献
Ferreira, Sabrina Baptista; Kaiser, Carlos Roland; Ferreira, Vitor Francisco
Organic Preparations and Procedures International, 2009 , vol. 41, # 3 p. 211 - 215
反应条件
ammonium cerium (IV) nitrate in ethylene glycol dimethyl ether; water T=20°C; 8 h; Inert atmosphere;
参考文献
Wang, Xue; Chen, Ye; Lee, Yong Rok
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 1 p. 153 - 156
反应条件
1: 98 percent / phenylboronic acid / acetic acid; toluene / 4 h / Heating 2: 100 percent / H2 / 10 percent Pd/C / ethyl acetate / 1 h / 2068.59 Torr 3: 62 percent / cerrium ammonium nitrate; H2O / acetonitrile / 0.5 h / 0 - 5 °C View Scheme
参考文献
Wang, Xue; Chen, Ye; Lee, Yong Rok
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 1 p. 153 - 156
反应条件
1: 98 percent / phenylboronic acid / acetic acid; toluene / 4 h / Heating 2: 100 percent / H2 / 10 percent Pd/C / ethyl acetate / 1 h / 2068.59 Torr 3: 62 percent / cerrium ammonium nitrate; H2O / acetonitrile / 0.5 h / 0 - 5 °C View Scheme
参考文献
Wang, Xue; Chen, Ye; Lee, Yong Rok
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 1 p. 153 - 156