2-羟甲基-1,3-丙二醇合成路线 （共 16 条）
反应条件
lipase from Pseudomonas stutzeri PS59 in aq. phosphate buffer; isopropyl alcohol T=30°C; pH=8; 0.25 h; Enzymatic reaction;
参考文献
Li, Xiao-Lu; Zhang, Wen-Hui; Wang, Ying-Dong; Dai, Yu-Jie; Zhang, Hui-Tu; Wang, Yue; Wang, Hai-Kuan; Lu, Fu-Ping
Journal of Molecular Catalysis B: Enzymatic, 2014 , vol. 102, p. 16 - 24
反应条件
lipase from Pseudomonas stutzeri PS59 in aq. phosphate buffer; isopropyl alcohol T=30°C; pH=8; 0.25 h; Enzymatic reaction;
参考文献
Li, Xiao-Lu; Zhang, Wen-Hui; Wang, Ying-Dong; Dai, Yu-Jie; Zhang, Hui-Tu; Wang, Yue; Wang, Hai-Kuan; Lu, Fu-Ping
Journal of Molecular Catalysis B: Enzymatic, 2014 , vol. 102, p. 16 - 24
反应条件
lipase from Pseudomonas stutzeri PS59 in aq. phosphate buffer; isopropyl alcohol T=30°C; pH=8; 0.25 h; Enzymatic reaction;
参考文献
Li, Xiao-Lu; Zhang, Wen-Hui; Wang, Ying-Dong; Dai, Yu-Jie; Zhang, Hui-Tu; Wang, Yue; Wang, Hai-Kuan; Lu, Fu-Ping
Journal of Molecular Catalysis B: Enzymatic, 2014 , vol. 102, p. 16 - 24
反应条件
hydrogen; ruthenium in water T=25°C; P=2585.7 Torr; 24 h; Yield given;
参考文献
Thiokol Corporation
Patent: US4336408 A1, 1982 ;
反应条件
water; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in acetonitrile T=20°C; 5 h;
参考文献
Liu, Junjie; Wong, Chi-Huey
Tetrahedron Letters, 2002 , vol. 43, # 22 p. 4037 - 4039
反应条件
sodium methylate in methanol 20 h; Heating;
参考文献
Latour, Stephan; Wuest, James D.
Synthesis, 1987 , # 8 p. 742 - 744
反应条件
dimethylsulfide borane complex 1.) reflux, 8 h, 2.) methanol, 15 h;
参考文献
Harnden; Wyatt; Boyd; Sutton
Journal of Medicinal Chemistry, 1990 , vol. 33, # 1 p. 187 - 196
反应条件
sulfuric acid; hydrogen; iron(II) sulfate; palladium on activated charcoal; Ru-carbon 1.) 25 deg C, 5 h, 2.) 50 psi, 25 deg C, 42 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Nielsen, Arnold T.; Moore, Donald W.; Schuetze, Bryan D.
Polish Journal of Chemistry, 1981 , vol. 55, # 6 p. 1393 - 1403
反应条件
sodium hydroxide; sulfuric acid; hydrogen; 5 activated charcoal-supported ruthenium catalyst 1.) 25 deg C, 30 min, 2.) 50 psi, 25 deg C, 4 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Nielsen, Arnold T.; Moore, Donald W.; Schuetze, Bryan D.
Polish Journal of Chemistry, 1981 , vol. 55, # 6 p. 1393 - 1403
反应条件
calcium hydroxide powder Mechanism;
参考文献
Werle, Peter; Busker, Eberhard; Wolf-Heuss, Elisabeth
Liebigs Annalen der Chemie, 1985 , # 5 p. 1082 - 1087
