1,4-二氧杂螺[4.5]癸-6-烯-8-酮合成路线 (共 2 条)
反应条件
1: tert-butyl alcohol / 45 h / |Irradiation; |Inert atmosphere 2: potassium carbonate / 3 h / 42 °C View Scheme
参考文献
Chen, Yu-Jen; Wang, Hui-Ling; Villarante, Nelson R.; Chuang, Gary Jing; Liao, Chun-Chen
Tetrahedron, 2013 , vol. 69, # 46 p. 9591 - 9599
反应条件
1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0.5 h / 0 °C
2: oxalic acid / methanol; water / 0.5 h
3: 2,2,2-trifluoroethanol / 40 h / |Irradiation; |Inert atmosphere
View Scheme
参考文献
Chen, Yu-Jen; Wang, Hui-Ling; Villarante, Nelson R.; Chuang, Gary Jing; Liao, Chun-Chen
Tetrahedron, 2013 , vol. 69, # 46 p. 9591 - 9599