CBZ-GLU(OME)-OH合成路线 (共 22 条)
反应条件
sodium carbonate in 1,4-dioxane Ambient temperature;
参考文献
Feng, Xianqi; Edstrom, Eric D.
Tetrahedron Asymmetry, 1999 , vol. 10, # 1 p. 99 - 105
反应条件
triethylamine; 4-(N,N-dimethlyamino)pyridine in dichloromethane T=0°C; 2 h; without cat., 2h; Yields of byproduct given;
参考文献
Jouin, P.; Castro, B.; Zeggaf, C.; Pantaloni, A.; Senet, J.P; et al
Tetrahedron Letters, 1987 , vol. 28, # 15 p. 1665 - 1668
反应条件
triethylamine; 4-(N,N-dimethlyamino)pyridine in dichloromethane T=0°C; 1 h; without cat., 2h; Yields of byproduct given;
参考文献
Jouin, P.; Castro, B.; Zeggaf, C.; Pantaloni, A.; Senet, J.P; et al
Tetrahedron Letters, 1987 , vol. 28, # 15 p. 1665 - 1668
反应条件
triethylamine; 4-(N,N-dimethlyamino)pyridine in dichloromethane T=0°C; 1 h; without DMAP; Yields of byproduct given;
参考文献
Nutt, Ruth F.; Strachan, Robert G.; Veber, Daniel F.; Holly, Frederick W.
Journal of Organic Chemistry, 1980 , vol. 45, # 15 p. 3078 - 3080
反应条件
potassium carbonate in water; acetone 1.5 h; Ambient temperature;
参考文献
Del Bosco, Marco; Johnstone, Andrew N.C.; Bazza, Giorgia; Lopatriello, Stefania; North, Michael
Tetrahedron, 1995 , vol. 51, # 31 p. 8545 - 8554
反应条件
1: SOCl2 2: NaHCO3 / toluene; H2O View Scheme
参考文献
Hanby et al.
Journal of the Chemical Society, 1950 , p. 3239,3243
反应条件
CaCl T=35°C; α-chymotrypsin A, McIlvaine buffer; Yield given;
参考文献
Shin, Chung-gi; Seki, Masashi; Takahashi, Nobuyuki
Chemistry Letters, 1990 , # 11 p. 2089 - 2090
反应条件
magnesium oxide; benzyl chloroformate
参考文献
Hanby et al.
Journal of the Chemical Society, 1950 , p. 3239,3243
反应条件
1: acetic acid anhydride 2: methanol View Scheme
参考文献
Le Quesne; Young
Journal of the Chemical Society, 1950 , p. 1954,1958
参考文献
Klieger,E.; Gibian,H.
Justus Liebigs Annalen der Chemie, 1962 , vol. 655, p. 195 - 210
Full Text Show Details
Le Quesne; Young
Journal of the Chemical Society, 1950 , p. 1954,1958