N,N-二乙基氨基甲酸甲酯合成路线 (共 17 条)
反应条件
sodium hydroxide in water
参考文献
Baum,K.; Beard,C.D.
Journal of Organic Chemistry, 1975 , vol. 40, p. 81 - 85
反应条件
1: phosgene; triethylamine in dichloromethane; toluene
T=20°C; 8 h;
2: methanol in dichloromethane; toluene
T=20°C;
参考文献
Itaya, Taisuke; Kanai, Tae
Chemical and Pharmaceutical Bulletin, 2002 , vol. 50, # 12 p. 1584 - 1588
反应条件
DAST
0.25 h; Heating;
参考文献
Dmowski,W.; Kaminski,M.
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 219
反应条件
4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane in tetrahydrofuran
15 h; Ambient temperature;
参考文献
Belforte, Antonio; Calderazzo, Fausto
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1989 , p. 1007 - 1010
反应条件
4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane in tetrahydrofuran
15 h; Ambient temperature;
参考文献
Belforte, Antonio; Calderazzo, Fausto
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1989 , p. 1007 - 1010
反应条件
T=120°C; P=30400 Torr; 45 h;
参考文献
Ishii, Shideru; Nakayama, Hidenobu; Yoshida, Yasuhiko; Yamashita, Tadataka
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 2 p. 455 - 458
反应条件
in tetrachloromethane
参考文献
Baum,K.; Beard,C.D.
Journal of Organic Chemistry, 1975 , vol. 40, p. 81 - 85
反应条件
T=120°C; P=30400 Torr; 45 h;
参考文献
Ishii, Shideru; Nakayama, Hidenobu; Yoshida, Yasuhiko; Yamashita, Tadataka
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 2 p. 455 - 458
参考文献
Ried; Hillenbrand
Justus Liebigs Annalen der Chemie, 1954 , vol. 590, p. 128,133
参考文献
Shramova,Z.I.; Skoldinov,A.P.
Zhurnal Organicheskoi Khimii, 1965 , vol. 1, p. 1743 - 1747,1775 - 1778