苯并[g]异喹啉-5,10-二酮合成路线 （共 19 条）
反应条件
2,2,6,6-tetramethylpiperidinyl-lithium in tetrahydrofuran; hexane T=20°C; 2 h;
参考文献
Rebstock, Anne-Sophie; Mongin, Florence; Trecourt, Francois; Queguiner, Guy
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 3 p. 291 - 295
反应条件
1: With hydrogenchloride in diethyl ether T=20°C; 16 h; 2: With air; sodium hydrogencarbonate in diethyl ether; water Further stages.;
参考文献
Jacobs, Jan; Kesteleyn, Bart; De Kimpe, Norbert
Tetrahedron, 2008 , vol. 64, # 22 p. 4985 - 4992
反应条件
hydrogen bromide; acetic acid T=20°C; 16 h;
参考文献
Jacobs, Jan; Kesteleyn, Bart; De Kimpe, Norbert
Tetrahedron, 2008 , vol. 64, # 22 p. 4985 - 4992
反应条件
T=150 - 160°C; 0.166667 h;
参考文献
Potts, Kevin T.; Bhattacharjee, Debkumar; Walsh, Eileen B.
Journal of Organic Chemistry, 1986 , vol. 51, # 11 p. 2011 - 2021
反应条件
sulfuric acid T=220°C; 0.5 h;
参考文献
Artamonov, A. A.; Shneider, T.; Baranova, N. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 4 p. 397 - 401
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , vol. 16, # 4 p. 514 - 518
反应条件
1: 86 percent / conc. H2SO4, KNO3 / 6 h / 50 °C 2: 79 percent / activated carbon, FeCl3*6H2O, hydrazine / methanol / 16 h / Heating 3: 1.) Na2CO3, diazotized sulfanilic acid, 2.) sodium hydroxide, sodium dithionite / 1.) AcOH, 7-9 deg C, 30 min, 2.) water, 60 deg C, 30 min 4: 40 percent / 12 N H2SO4, 10percent potassium dichromate / CHCl3 / 0.17 h 5: benzene / 48 h / Heating View Scheme
参考文献
Potts, Kevin T.; Bhattacharjee, Debkumar; Walsh, Eileen B.
Journal of Organic Chemistry, 1986 , vol. 51, # 11 p. 2011 - 2021
反应条件
1: 1.) Na2CO3, diazotized sulfanilic acid, 2.) sodium hydroxide, sodium dithionite / 1.) AcOH, 7-9 deg C, 30 min, 2.) water, 60 deg C, 30 min 2: 40 percent / 12 N H2SO4, 10percent potassium dichromate / CHCl3 / 0.17 h 3: benzene / 48 h / Heating View Scheme
参考文献
Potts, Kevin T.; Bhattacharjee, Debkumar; Walsh, Eileen B.
Journal of Organic Chemistry, 1986 , vol. 51, # 11 p. 2011 - 2021
反应条件
1: 79 percent / activated carbon, FeCl3*6H2O, hydrazine / methanol / 16 h / Heating 2: 1.) Na2CO3, diazotized sulfanilic acid, 2.) sodium hydroxide, sodium dithionite / 1.) AcOH, 7-9 deg C, 30 min, 2.) water, 60 deg C, 30 min 3: 40 percent / 12 N H2SO4, 10percent potassium dichromate / CHCl3 / 0.17 h 4: benzene / 48 h / Heating View Scheme
参考文献
Potts, Kevin T.; Bhattacharjee, Debkumar; Walsh, Eileen B.
Journal of Organic Chemistry, 1986 , vol. 51, # 11 p. 2011 - 2021
反应条件
1: 40 percent / 12 N H2SO4, 10percent potassium dichromate / CHCl3 / 0.17 h 2: benzene / 48 h / Heating View Scheme
参考文献
Potts, Kevin T.; Bhattacharjee, Debkumar; Walsh, Eileen B.
Journal of Organic Chemistry, 1986 , vol. 51, # 11 p. 2011 - 2021
反应条件
1: benzene / 24 h / Heating 2: 68 percent / Ag2O / 1,2-dimethoxy-ethane / 6 h / Ambient temperature 3: 80 percent / 0.17 h / 150 - 160 °C View Scheme
参考文献
Potts, Kevin T.; Bhattacharjee, Debkumar; Walsh, Eileen B.
Journal of Organic Chemistry, 1986 , vol. 51, # 11 p. 2011 - 2021
