in chloroform-d1 allowing soln. of greatest (total tfa)/(total Co) to stand either in diffuse daylight or in the dark at room temp. for 1-2 d; crystals filtered off, washed with cold solvent and hexane, air-dried, dried in vac. at 10-12 mmHg for a few hours;
参考文献
Alcock, Nathaniel W.; Atkins, Martin P.; Golding, Bernard T.; Sellars, Philip J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1982 , p. 337 - 344
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反应条件
in chloroform-d1 allowing soln. of greatest (total tfa)/(total Co) to stand either in diffuse daylight or in the dark at room temp. for 1-2 d; crystals filtered off, washed with cold solvent and hexane, air-dried, dried in vac. at 10-12 mmHg for a few hours;
参考文献
Alcock, Nathaniel W.; Atkins, Martin P.; Golding, Bernard T.; Sellars, Philip J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1982 , p. 337 - 344
