反应条件
1.1: 3-chloro-benzenecarboperoxoic acid; sodium hydrogencarbonate / dichloromethane / 40 h / 20 °C / |Inert atmosphere 2.1: titanium (IV) bromide / dichloromethane / 72 h / 20 °C / |Inert atmosphere 2.2: 5.5 h / -10 - 20 °C / |Inert atmosphere 3.1: potassium tert-butylate / water; dimethyl sulfoxide / 2 h / 20 °C / |Inert atmosphere 3.2: pH 2 / |Cooling with ice View Scheme
参考文献
Krief, Alain; Jeanmart, Stephane; Gondal, Humaira Y.; Kremer, Adrian
Helvetica Chimica Acta, 2012 , vol. 95, # 11 p. 2123 - 2167