1: 1-bromo-2-phenylbenzene With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 1 h;
2: acetone in tetrahydrofuran; hexane
T=-78 - 20°C; Further stages.;
参考文献
Casarini, Daniele; Lunazzi, Lodovico; Mancinelli, Michele; Mazzanti, Andrea; Rosini, Carlo
Journal of Organic Chemistry, 2007 , vol. 72, # 20 p. 7667 - 7676
Bradsher; Amore
Journal of the American Chemical Society, 1943 , vol. 65, p. 2016
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Mowry et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 1916
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Monsanto Chem. Co.
Patent: GB633646 , 1947 ;
palladium diacetate; caesium carbonate; triphenylphosphine in o-xylene
15 h; Heating; Further byproducts given. Title compound not separated from byproducts;
参考文献
Terao; Wakui; Satoh; Miura; Nomura
Journal of the American Chemical Society, 2001 , vol. 123, # 42 p. 10407 - 10408
palladium diacetate; caesium carbonate; triphenylphosphine in o-xylene
15 h; Heating; Further byproducts given. Title compound not separated from byproducts;
参考文献
Terao; Wakui; Satoh; Miura; Nomura
Journal of the American Chemical Society, 2001 , vol. 123, # 42 p. 10407 - 10408
