3-(4-甲基苯甲酰)丙酸合成路线 (共 57 条)
反应条件
hydrogen; palladium in methanol T=20°C; 10 h;
参考文献
Ikawa, Takashi; Sajiki, Hironao; Hirota, Kosaku
Tetrahedron, 2005 , vol. 61, # 8 p. 2217 - 2231
反应条件
aluminium trichloride T=60°C; 1 h;
参考文献
Kim, Choung Un; Misco, Peter F.; Luh, Bing Y.; Mansuri, Muzammil M.
Tetrahedron Letters, 1994 , vol. 35, # 19 p. 3017 - 3020
反应条件
sodium hydroxide in ethanol; water 1 h; Heating;
参考文献
Bhat, K. S.; Rao, A. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 5 p. 355 - 358
参考文献
Bhat, K. S.; Rao, A. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 5 p. 355 - 358
反应条件
1: 31 percent / NaBH4, NaHCO3 / methanol; H2O / 1.5 h / 28 °C 2: 78 percent / NaOH / ethanol; H2O / 1 h / Heating View Scheme
参考文献
Bhat, K. S.; Rao, A. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 5 p. 355 - 358
反应条件
hydrogenchloride; formaldehyd in 1,4-dioxane
参考文献
Severin,T.; Poehlmann,H.
Chemische Berichte, 1978 , vol. 111, p. 1564 - 1577
反应条件
1: NaBH4 / methanol; H2O / 1.) 5-10 deg C, 30 min , 2.) RT , 1 h 2: 78 percent / NaOH / ethanol; H2O / 1 h / Heating View Scheme
参考文献
Bhat, K. S.; Rao, A. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 5 p. 355 - 358
参考文献
Potikha; Lysakovskii; Kovtunenko; Turov
Russian Journal of Organic Chemistry, 2009 , vol. 45, # 12 p. 1818 - 1823
反应条件
hydrogenchloride 1.) THF, 66 deg C, 2 h, 2.) THF; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rahman, M. T.; Nur, H. P.
Journal of the Indian Chemical Society, 1994 , vol. 71, # 6-8 p. 469 - 474
参考文献
Katzenellenbogen
Chemische Berichte, 1901 , vol. 34, p. 3828
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Borsche
Chemische Berichte, 1914 , vol. 47, p. 1113