N-(噻吩-2-甲基)苯甲酰胺合成路线 （共 5 条）
反应条件
dicobalt octacarbonyl; hydrogen; Sb(o-tolyl)3 in tetrahydrofuran
T=120°C; P=33615.5 Torr; 24 h;
参考文献
Rubio-Perez, Laura; Sharma, Pankaj; Perez-Flores, F. Javier; Velasco, Luis; Arias, J. Luis.; Cabrera, Armando
Tetrahedron, 2012 , vol. 68, # 10 p. 2342 - 2348
反应条件
palladium diacetate; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in CPME; water
T=85°C; Suzuki-Miyaura cross-coupling; 6 h; Inert atmosphere;
参考文献
Molander, Gary A.; Hiebel, Marie-Aude
Organic Letters, 2010 , vol. 12, # 21 p. 4876 - 4879
参考文献
Hartough et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 1146,4013
参考文献
Hartough et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 4013,4017
反应条件
1.1: [Ir(μ-Cl)(cyclooctene)2]2; diethylesilane / 2 h / 80 °C / Inert atmosphere
2.1: hydrogenchloride / diethyl ether / 1 h / 23 °C / Inert atmosphere
2.2: 2 h / 23 °C / Inert atmosphere
View Scheme
参考文献
Cheng, Chen; Brookhart, Maurice
Journal of the American Chemical Society, 2012 , vol. 134, # 28 p. 11304 - 11307
