反应条件
1: 63 percent / NaH / tetrahydrofuran / 0.5 h / Heating
2: NaBH4 / methanol; tetrahydrofuran / 2 h / 4 - 7 °C
3: BF3*Et2O; MgSO4 / CH2Cl2 / 5 h / 20 °C
4: H2 / Pd(OH)2/C / acetic acid / 3 h / 20 °C
5: Na/Hg; Na3PO4 / methanol / 2 h / 20 °C
6: 92 percent / LiAlH4 / tetrahydrofuran / 2 h / Heating
View Scheme
参考文献
Chang, Meng-Yang; Chen, Shui-Tein; Chang, Nein-Chen
Tetrahedron, 2002 , vol. 58, # 18 p. 3623 - 3628
