1,3,5-三乙酰基-2-脱氧-D-赤式戊呋喃糖合成路线 （共 6 条）
反应条件
perchloric acid immobilized on silica gel in dichloromethane 4 h; Reflux;
参考文献
Du, Ti-Jian; Wu, Qin-Pei; Liu, Hai-Xia; Chen, Xi; Shu, Yi-Nan; Xi, Xiao-Dong; Zhang, Qing-Shan; Li, Yun-Zheng
Tetrahedron, 2011 , vol. 67, # 6 p. 1096 - 1101
反应条件
pyridine in 1,4-dioxane 3 h; Reflux;
参考文献
Zhou, Yue; Yu, Peilin; Jin, Hongwei; Yang, Zhenjun; Yue, Jianbo; Zhang, Liangren; Zhang, Lihe
Molecules, 2012 , vol. 17, # 4 p. 4343 - 4356
反应条件
sulfuric acid; acetic acid T=6 - 20°C; 5.66 h; Inert atmosphereIndustry scale;
参考文献
JOHNSON MATTHEW PUBLIC LIMITED COMPANY; FU, Xing; ZUMBRUNN, Albercht
Patent: WO2012/71508 A1, 2012 ;
Location in patent: Page/Page column 4; 9-10 ;
参考文献
Taverna-Porro, Marisa; Bouvier, Leon A.; Pereira, Claudio A.; Montserrat, Javier M.; Iribarren, Adolfo M.
Tetrahedron Letters, 2008 , vol. 49, # 16 p. 2642 - 2645
反应条件
1.1: hydrogenchloride / diethyl ether / 20 °C 1.2: 28 h / 20 °C 2.1: pyridine / dichloromethane / 7.97 h / -30 - 20 °C / Inert atmosphere; Industry scale 3.1: sulfuric acid; acetic acid / 5.66 h / 6 - 20 °C / Inert atmosphere; Industry scale View Scheme
参考文献
JOHNSON MATTHEW PUBLIC LIMITED COMPANY; FU, Xing; ZUMBRUNN, Albercht
Patent: WO2012/71508 A1, 2012 ;
反应条件
pyridine 25 h; Ambient temperature;
参考文献
Martinez, Heike Otero; Reinke, Helmut; Michalik, Dirk; Vogel, Christian
Synthesis, 2009 , # 11 art. no. T01909SS, p. 1834 - 1840
