(1S,4R)-N-羟基-7,7-二甲基-2-氧代双环[2.2.1]庚烷-1-甲酰胺合成路线 （共 2 条）
反应条件
1.1: 78 percent / Et4N(1+)*IO4(1-) / CH2Cl2 / 6 h / -78 °C 2.1: LiAlH4 / tetrahydrofuran / 0 - 20 °C 2.2: aq. HCl / diethyl ether 3.1: 310 mg / Jones reagent / acetone / 0 °C View Scheme
参考文献
Wang, Ying-Chuan; Lu, Tzung-Min; Elango, Shanmugham; Lin, Chao-Kuo; Tsai, Chia-Tzung; Yan, Tu-Hsin
Tetrahedron Asymmetry, 2002 , vol. 13, # 7 p. 691 - 695
反应条件
1.1: 78 percent / Et4N(1+)*IO4(1-) / CH2Cl2 / 6 h / -78 °C 2.1: LiAlH4 / tetrahydrofuran / 0 - 20 °C 2.2: aq. HCl / diethyl ether 3.1: 310 mg / Jones reagent / acetone / 0 °C View Scheme
参考文献
Wang, Ying-Chuan; Lu, Tzung-Min; Elango, Shanmugham; Lin, Chao-Kuo; Tsai, Chia-Tzung; Yan, Tu-Hsin
Tetrahedron Asymmetry, 2002 , vol. 13, # 7 p. 691 - 695
