4-甲基偶氮苯四氟硼酸盐合成路线 (共 216 条)
反应条件
water in acetonitrile
T=30°C; further reaction with 2-naphthylamine; effect of further catalysts; Rate constant;
参考文献
Penton, John R.; Zollinger, Heinrich
Helvetica Chimica Acta, 1981 , vol. 64, # 6 p. 1717 - 1727
反应条件
in dimethyl sulfoxide
0.666667 h;
参考文献
Petrillo, Giovanni; Novi, Marino; Garbarino, Giacomo; Filiberti, Marcos
Tetrahedron Letters, 1988 , vol. 29, # 33 p. 4185 - 4188
反应条件
2,6-di-tert-butyl-4-methylpyridine; gold(I) chloride; palladium dichloride; SIDip*HCl in acetonitrile
T=20°C; Sonogashira coupling;
参考文献
Panda, Biswajit; Sarkar, Tarun K.
Chemical Communications, 2010 , vol. 46, # 18 p. 3131 - 3133
反应条件
ammonia in acetone
molar ratio Bi:p-CH3C6H4N2BF4 = 2:1, cooling; addn. of diluted aq. NH3, extraction with benzene;
参考文献
Gmelin Handbook: Bi: Org.Verb., 1.3.3.2.6.1, page 82 - 86
反应条件
dibenzo-18-crown-6; Cu(BF4)2 in acetonitrile
T=20°C; Sandmeyer cyanation; 0.333333 h;
参考文献
Beletskaya, Irina P.; Sigeev, Alexander S.; Peregudov, Alexander S.; Petrovskii, Pavel V.
Journal of Organometallic Chemistry, 2004 , vol. 689, # 23 p. 3810 - 3812
反应条件
CuCN in acetone
T=15°C; Yield given. Yields of byproduct given;
参考文献
Obushak; Ganushchak; Matiichuk
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 5 p. 766 - 766