2-乙酰基-2-甲基环氧乙烷合成路线 （共 10 条）
反应条件
2: H2 / Raney-Ni / dioxane View Scheme
参考文献
Tishchenko,I.G.; Malashko,P.M.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1966 , vol. 2, p. 357 - 360
Khimiya Geterotsiklicheskikh Soedinenii, 1966 , vol. 2, p. 483 - 486
反应条件
perchloric acid; dihydrogen peroxide in water; acetonitrile; tert-butyl alcohol
T=60°C; 1 h; stereoselective reaction;
参考文献
Mizuno, Noritaka; Kamata, Keigo; Yamaguchi, Kazuya
Catalysis Today, 2012 , vol. 185, # 1 p. 157 - 161
反应条件
triphenylphosphine in dichloromethane
1 h; Heating;
参考文献
Griesbaum, Karl; Keul, Helmut; Agarwal, Sudhir; Zwick, Gerhard
Chemische Berichte, 1983 , vol. 116, # 2 p. 409 - 415
反应条件
in diethyl ether
T=-85°C; 1 h; Inert atmosphere;
参考文献
Lo, Brian; Chiu, Pauline
Organic Letters, 2011 , vol. 13, # 5 p. 864 - 867
反应条件
in diethyl ether
T=20°C;
参考文献
Hartung, Ryan E.; Paquette, Leo A.
Heterocycles, 2004 , vol. 64, p. 23 - 26
反应条件
1: 73 percent / MCPB / CH2Cl2 / 24 h / Ambient temperature
2: 91 percent / P(Ph)3 / CH2Cl2 / 1 h / Heating
View Scheme
参考文献
Griesbaum, Karl; Keul, Helmut; Agarwal, Sudhir; Zwick, Gerhard
Chemische Berichte, 1983 , vol. 116, # 2 p. 409 - 415
反应条件
boric acid
Heating; Yield given;
参考文献
Bubel, O. N.; Tishchenko, I. G.; Stasevich, G. Z.; Veraksich, E. L.; Filich, E. R.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1985 , vol. 21, # 9 p. 1082 - 1085
Khimiya Geterotsiklicheskikh Soedinenii, 1985 , vol. 21, # 9 p. 1322 - 1326
反应条件
boron trifluoride in dichloromethane
T=0 - 5°C; 1 h; Yields of byproduct given;
参考文献
Bubel', O. N.; Tishchenko, I. G.; Ptashnikov, Yu. L.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 8 p. 773 - 775
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 8 p. 1022 - 1024
反应条件
boron trifluoride diethyl etherate
Yields of byproduct given;
参考文献
Bubel', O. N.; Tishchenko, I. G.; Ptashnikov, Yu. L.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 8 p. 773 - 775
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 8 p. 1022 - 1024
反应条件
sodium hydroxide in methanol
参考文献
Koval'chuk; Kuz'menok; Zvonok
Chemistry of Heterocyclic Compounds, 2005 , vol. 41, # 10 p. 1237 - 1244
