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乙二醇
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63148-62-9
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碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4568-88-1
合成路线
（共 11 条）
4568-88-1
→
反应条件
18270-60-5
反应条件
1: lead (IV)-acetate; acetic acid 2: Raney nickel; ethanol / 100 °C / 73550.8 Torr / Hydrogenation 3: ethanol; hydrazine hydrate View Scheme
参考文献
Lemieux
Canadian Journal of Chemistry, 1953 , vol. 31, p. 396,414
4568-88-1
→
反应条件
4617-33-8
15-羟基十五酸
反应条件
1: lead (IV)-acetate; acetic acid 2: Raney nickel; ethanol / 100 °C / 73550.8 Torr / Hydrogenation 3: alkaline solution View Scheme
参考文献
Lemieux
Canadian Journal of Chemistry, 1953 , vol. 31, p. 396,414
488117-69-7
→
反应条件
4568-88-1
反应条件
acetic acid in tetrahydrofuran T=60°C; 5 h;
参考文献
Liu, Hai-Xia; Huang, Guo-Rui; Zhang, Huan-Ming; Wu, Jia-Rui; Yao, Zhu-Jun
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 12 p. 3426 - 3430
7735-38-8
13-羟基十三烷酸
→
反应条件
4568-88-1
反应条件
1: HBr; HOAc 2: SOCl2 3: t-BuOK 4: H2 / Pd/C / ethanol / 760.05 Torr 5: 94 percent / HOAc / tetrahydrofuran View Scheme
参考文献
Liu, Hai-Xia; Huang, Guo-Rui; Zhang, Huan-Ming; Wu, Jia-Rui; Yao, Zhu-Jun
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 12 p. 3426 - 3430
112-86-7
芥酸
→
反应条件
4568-88-1
反应条件
1: O3 / ethanol; cyclohexane / 0 - 5 °C 2: KBH4 3: HBr; HOAc 4: SOCl2 5: t-BuOK 6: H2 / Pd/C / ethanol / 760.05 Torr 7: 94 percent / HOAc / tetrahydrofuran View Scheme
参考文献
Liu, Hai-Xia; Huang, Guo-Rui; Zhang, Huan-Ming; Wu, Jia-Rui; Yao, Zhu-Jun
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 12 p. 3426 - 3430
80982-86-1
→
反应条件
4568-88-1
反应条件
1: t-BuOK 2: H2 / Pd/C / ethanol / 760.05 Torr 3: 94 percent / HOAc / tetrahydrofuran View Scheme
参考文献
Liu, Hai-Xia; Huang, Guo-Rui; Zhang, Huan-Ming; Wu, Jia-Rui; Yao, Zhu-Jun
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 12 p. 3426 - 3430
7147-29-7
→
反应条件
4568-88-1
反应条件
1.1: 92 percent / CBr4; PPh3 / benzene / 2.33 h / 20 °C 2.1: 5 h / 80 °C 3.1: tBuOK / tetrahydrofuran / 0.17 h / -50 - -40 °C 3.2: tetrahydrofuran / 2 h / -70 °C 4.1: H2 / 10percent Pd/C / methanol 5.1: 94 percent / aq. AcOH / tetrahydrofuran / 5 h / 60 °C View Scheme
参考文献
Zeng, Bu-Bing; Wu, Yikang; Jiang, Sheng; Yu, Qian; Yao, Zhu-Jun; Liu, Zhong-Hai; Li, Hong-Yan; Li, Yan; Chen, Xiao-Guang; Wu, Yu-Lin
Chemistry - A European Journal, 2003 , vol. 9, # 1 p. 282 - 290
488117-68-6
→
反应条件
4568-88-1
反应条件
1: H2 / Pd/C / ethanol / 760.05 Torr 2: 94 percent / HOAc / tetrahydrofuran View Scheme
参考文献
Liu, Hai-Xia; Huang, Guo-Rui; Zhang, Huan-Ming; Wu, Jia-Rui; Yao, Zhu-Jun
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 12 p. 3426 - 3430
15462-16-5
→
反应条件
4568-88-1
反应条件
1: SOCl2 2: t-BuOK 3: H2 / Pd/C / ethanol / 760.05 Torr 4: 94 percent / HOAc / tetrahydrofuran View Scheme
参考文献
Liu, Hai-Xia; Huang, Guo-Rui; Zhang, Huan-Ming; Wu, Jia-Rui; Yao, Zhu-Jun
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 12 p. 3426 - 3430
65157-88-2
→
反应条件
4568-88-1
反应条件
1: KBH4 2: HBr; HOAc 3: SOCl2 4: t-BuOK 5: H2 / Pd/C / ethanol / 760.05 Torr 6: 94 percent / HOAc / tetrahydrofuran View Scheme
参考文献
Liu, Hai-Xia; Huang, Guo-Rui; Zhang, Huan-Ming; Wu, Jia-Rui; Yao, Zhu-Jun
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 12 p. 3426 - 3430
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