2-氯-3-(氯甲基)吡嗪合成路线 （共 5 条）
反应条件
trichloroisocyanuric acid; benzamide in chloroform Reflux;
参考文献
Gavardinas, Konstantinos; Green, Jonathan Edward; Jadhav, Prabhakar Kondaji; Matthews, Donald Paul
Patent: US2010/69404 A1, 2010 ;
Location in patent: Page/Page column 15 ;
反应条件
1: With thionyl chloride; N,N-dimethyl-formamide in toluene T=40°C; 0.666667 h; 2: With sodium carbonate in water; toluene pH=7;
参考文献
Mulvihill, Kristen Michelle; Castelhano, Arlindo L.
Patent: US2007/129547 A1, 2007 ;
Location in patent: Page/Page column 3-4 ;
反应条件
trichlorophosphate 16 h; Heating;
参考文献
Sato, Nobuhiro
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 149 - 152
反应条件
trichlorophosphate T=180 - 185°C; 3 h; Product distributionMechanism;
参考文献
Sato, Nobuhiro
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 149 - 152
反应条件
in N,N-dimethyl-formamide
T=60°C; 17 h;
参考文献
Mulvihill, Kristen Michelle; Castelhano, Arlindo L.
Patent: US2007/129547 A1, 2007 ;
Location in patent: Page/Page column 4 ;
