4-(三氟甲氧基)苯甲酰胺合成路线 （共 17 条）
反应条件
toluene-4-sulfonic acid; 1,2-bis-(diphenylphosphino)ethane; carbonyl(dihydro)tris(triphenylphosphine)ruthenium(II) in toluene Heating;
参考文献
Owston, Nathan A.; Parker, Alexandra J.; Williams, Jonathan M. J.
Organic Letters, 2007 , vol. 9, # 18 p. 3599 - 3601
反应条件
tert.-butylhydroperoxide; ammonium hydroxide in water T=100°C; 16 h;
参考文献
Wu, Xiao-Feng; Sharif, Muhammad; Feng, Jian-Bo; Neumann, Helfried; Pews-Davtyan, Anahit; Langer, Peter; Beller, Matthias
Green Chemistry, 2013 , vol. 15, # 7 p. 1956 - 1961
反应条件
in chloroform; water; 1,2-dichloro-ethane
参考文献
Sterling Drug Inc.
Patent: US3960945 A1, 1976 ;
反应条件
[Pd(η3-1-Ph-allyl)(μ-Cl)]2; nonafluoro-n-butanesulfonyl fluoride; ammonia; 1,8-diazabicyclo[5.4.0]undec-7-ene; bis[2-(diphenylphosphino)phenyl] ether in acetonitrile T=80°C; P=1500.15 Torr; 16 h; Inert atmosphereAutoclave;
参考文献
Wu, Xiao-Feng; Neumann, Helfried; Beller, Matthias
Chemistry - A European Journal, 2012 , vol. 18, # 2 p. 419 - 422
反应条件
Ru(DMSO)4Cl2; hydroxylamine hydrochloride; sodium hydrogencarbonate in acetonitrile T=78°C; 6 h; Inert atmosphere;
参考文献
Hull, Jonathan F.; Hilton, Sheena T.; Crabtree, Robert H.
Inorganica Chimica Acta, 2010 , vol. 363, # 6 p. 1243 - 1245
反应条件
ammonium hydroxide in ethyl acetate 0.166667 h;
参考文献
Weikert; Bingham Jr.; Emanuel; Fraser-Smith; Loughhead; Nelson; Poulton
Journal of Medicinal Chemistry, 1991 , vol. 34, # 5 p. 1630 - 1633
反应条件
1: (COCl)2, DMF / CH2Cl2 / Heating 2: conc. NH4OH / ethyl acetate / 0.17 h View Scheme
参考文献
Weikert; Bingham Jr.; Emanuel; Fraser-Smith; Loughhead; Nelson; Poulton
Journal of Medicinal Chemistry, 1991 , vol. 34, # 5 p. 1630 - 1633
参考文献
Jagupol'skii; Troizkaja
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 518,522; engl. Ausg. S. 587, 591
Full Text Show Details
Jagupol'skii
Doklady Akademii Nauk SSSR, 1955 , vol. 105, p. 100
Chem.Abstr., 1956 , p. 11270
反应条件
sodium hydroxide; dihydrogen peroxide
参考文献
Jagupol'skii; Troizkaja
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 518,522; engl. Ausg. S. 587, 591
反应条件
1: SbCl5; SbF3 2: aqueous NH3 View Scheme
参考文献
Jagupol'skii; Troizkaja
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 518,522; engl. Ausg. S. 587, 591
