4-硝基重氮苯四氟硼酸盐合成路线 （共 247 条）
反应条件
1: With hydrogenchloride; sodium nitrite in water T=0°C; 2: With sodium tetrafluoroborate in water
参考文献
Parola, Stephane; Desroches, Cedric; Vocanson, Francis; Bouix, Jean; Lamartine, Roger
Patent: US2004/127722 A1, 2004 ;
Location in patent: Page 7 ;
反应条件
sodium nitrite in water
参考文献
Prasad Hari, Durga; Hering, Thea; Koenig, Burkhard
Angewandte Chemie - International Edition, 2014 , vol. 53, # 3 p. 725 - 728
Angew. Chem., 2013 , vol. 126, # 3 p. 743 - 747,5
反应条件
in methanol T=25°C; Equilibrium constant;
参考文献
Izatt, R. M.; Lamb, J. D.; Swain, C. S.; Christensen, J. J.; Haymore, Barry L.
Journal of the American Chemical Society, 1980 , vol. 102, # 9 p. 3032 - 3034
反应条件
in water T=5°C; Cooling with ice;
参考文献
Raicopol, Matei; Branzoi, Viorel; Necula, Luiza; Ionita, Mariana; Pilan, Luisa
Revue Roumaine de Chimie, 2012 , vol. 57, # 9-10 p. 807 - 814
反应条件
in dimethyl sulfoxide Irradiation;
参考文献
Russell,G.A. et al.
Journal of the American Chemical Society, 1971 , vol. 93, p. 5839 - 5845
反应条件
chlorine in acetone ppt. is extd. with CHCl3, then addn. of Cl2; evapn. of CHCl3, recrystn. from acetone - ethanol;
参考文献
Nesmeyanov, A. N.; Tolstaya, T. P.; Isaeva, L. Sh.
Doklady Akademii Nauk SSSR, 1958 , vol. 122, p. 614 - 617
Full Text Show Details
Gmelin Handbook: Bi: Org.Verb., 1.3.1.2.2.3, page 21 - 25
反应条件
bismuth anschliessende Umsetzung mit Chlor;
参考文献
Nesmejanow et al.
Doklady Akademii Nauk SSSR, 1958 , vol. 122, p. 614,615
Doklady Chemistry, 118-123<1958>725
反应条件
copper(I) bromide; phosphorus trichoride
参考文献
Doak; Freedman
Journal of the American Chemical Society, 1951 , vol. 73, p. 5658
反应条件
magnesium 1.) THF, reflux, 2.) THF, 30 deg C, 90 s; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Singh, P. R.; Khanna, R. K.; Jayaraman, B.
Tetrahedron Letters, 1982 , vol. 23, # 51 p. 5475 - 5478
反应条件
in dimethyl sulfoxide T=20°C; Arylation; 1 h;
参考文献
Gurczynski, Marek; Tomasik, Piotr
Organic Preparations and Procedures International, 1991 , vol. 23, # 4 p. 438 - 441
