2-氯代-4'-氟苯乙酮合成路线 （共 49 条）
反应条件
chloro-trimethyl-silane; potassium nitrate in dichloromethane T=60°C; 48 h;
参考文献
Prakash, G.K. Sxurya; Ismail, Rehana; Garcia, Jessica; Panja, Chiradeep; Rasul, Golam; Mathew, Thomas; Olah, George A.
Tetrahedron Letters, 2011 , vol. 52, # 11 p. 1217 - 1221
反应条件
aluminium trichloride in carbon disulfide 2 h; Heating;
参考文献
Tichniouin; Sauleau; Lacroix
European Journal of Medicinal Chemistry, 1985 , vol. 20, # 2 p. 181 - 186
反应条件
S4N4*SbCl5 in toluene 3.5 h; Heating;
参考文献
Kim, Kil-Joong; Kim, Kyongtae
Tetrahedron Letters, 1997 , vol. 38, # 24 p. 4227 - 4230
反应条件
ruthenium (2+) in benzene T=120°C; 7 h; sealed;
参考文献
Kamigata, Nobumasa; Udodaira, Kumiko; Yoshikawa, Manabu; Shimizu, Toshio
Journal of Organometallic Chemistry, 1998 , vol. 552, # 1-2 p. 39 - 43
反应条件
in chloroform; [2-(4-fluorophenyl)-2-oxo]-ethyl 5-chloropyrid-2-yldithiocarbamate; acetonitrile
参考文献
Rhone-Poulenc Industries
Patent: US4271167 A1, 1981 ;
反应条件
pyridine; formic acid; chlorosulphonyl isocyanate in acetonitrile T=0 - 10°C; Inert atmosphere;
参考文献
Wang, You-Qing; Yu, Chang-Bin; Wang, Da-Wei; Wang, Xiao-Bing; Zhou, Yong-Gui
Organic Letters, 2008 , vol. 10, # 10 p. 2071 - 2074
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in benzene T=120°C; 7 h;
参考文献
Kamigata, Nobumasa; Udodaira, Kumiko; Shimizu, Toshio
Phosphorus, Sulfur and Silicon and Related Elements, 1997 , vol. 129, p. 155 - 168
反应条件
sodium hypochlorite T=40.8°C; μ=0.025, var. temp. and solvents; or in the presence of α- or β-cyclodextrin in var. conc.; ΔH(excit.), ΔS(excit.); Rate constantThermodynamic dataKinetics;
参考文献
Kamigata, Nobumasa; Udodaira, Kumiko; Yoshikawa, Manabu; Shimizu, Toshio
Journal of Organometallic Chemistry, 1998 , vol. 552, # 1-2 p. 39 - 43
反应条件
triethylamine in diethyl ether Inert atmosphere;
参考文献
Yagupolskii, Lev M.; Maletina, Irina I.; Sokolenko, Liubov V.; Vlasenko, Yurii G.; Drozdova, Maria V.; Polovinko, Vitaliy V.
Journal of Fluorine Chemistry, 2010 , vol. 131, # 2 p. 238 - 247
反应条件
triethylamine in tetrahydrofuran Inert atmosphere;
参考文献
Yagupolskii, Lev M.; Maletina, Irina I.; Sokolenko, Liubov V.; Vlasenko, Yurii G.; Drozdova, Maria V.; Polovinko, Vitaliy V.
Journal of Fluorine Chemistry, 2010 , vol. 131, # 2 p. 238 - 247
