3-氟-4-甲氧基苯乙酮合成路线 （共 20 条）
反应条件
1: acetyl chloride With AlCl3, aluminium chloride in chloroform T=5 - 10°C; 0.166667 h; 2: ortho-fluoroanisole in chloroform T=0 - 10°C; 1 h;
参考文献
G. D. Searle and Co.
Patent: US6342510 B1, 2002 ;
Location in patent: Page column 28 ;
反应条件
acetic anhydride; AlCl3
参考文献
Displaytech, Inc.
Patent: US5422037 A1, 1995 ;
参考文献
Yerande, Swapnil G.; Shendage, Deepak M.; Wakchaure, Prasad B.; Phadtare, Ganesh R.; Bhoite, Madhavrao Y.; Gangopadhyay, Ashok Kumar; Nagarajan, Kuppuswamy; Rupp, Richard Helmut
Tetrahedron Letters, 2014 , vol. 55, # 15 p. 2426 - 2429
反应条件
accufluorTM in acetonitrile T=80°C; 12 h;
参考文献
Stavber, Stojan; Zupan, Marko
Tetrahedron Letters, 1996 , vol. 37, # 20 p. 3591 - 3594
反应条件
carbon disulfide; aluminium trichloride
参考文献
English; Mead; Niemann
Journal of the American Chemical Society, 1940 , vol. 62, p. 350,353
反应条件
1: AlCl3 2: aqueous alkaline solution View Scheme
参考文献
Yerande, Swapnil G.; Shendage, Deepak M.; Wakchaure, Prasad B.; Phadtare, Ganesh R.; Bhoite, Madhavrao Y.; Gangopadhyay, Ashok Kumar; Nagarajan, Kuppuswamy; Rupp, Richard Helmut
Tetrahedron Letters, 2014 , vol. 55, # 15 p. 2426 - 2429
反应条件
1: thionyl chloride; acetic acid 2: AlCl3 3: aqueous alkaline solution View Scheme
参考文献
Yerande, Swapnil G.; Shendage, Deepak M.; Wakchaure, Prasad B.; Phadtare, Ganesh R.; Bhoite, Madhavrao Y.; Gangopadhyay, Ashok Kumar; Nagarajan, Kuppuswamy; Rupp, Richard Helmut
Tetrahedron Letters, 2014 , vol. 55, # 15 p. 2426 - 2429
参考文献
English; Mead; Niemann
Journal of the American Chemical Society, 1940 , vol. 62, p. 350,353
反应条件
in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; toluene
参考文献
Nippon Mining Co., Ltd.
Patent: US5098602 A1, 1992 ;
反应条件
aluminum tri-bromide in ethyl acetate; benzene
参考文献
Biorex Laboratories Limited
Patent: US4190671 A1, 1980 ;
