2-苯基-4-喹啉羧酸甲酯合成路线 (共 21 条)
反应条件
dicyclohexyl-carbodiimide; 4-(N,N-dimethlyamino)pyridine in dichloromethane
T=0 - 20°C; 13 h;
参考文献
Lautens, Mark; Tayama, Eiji; Herse, Christelle
Journal of the American Chemical Society, 2005 , vol. 127, # 1 p. 72 - 73
反应条件
anhydrous iron chloride; di-tert-butyl peroxide in 1,2-dichloro-ethane
T=80°C; 12 h; Schlenk technique;
参考文献
Liu, Peng; Li, Yuxi; Wang, Haiyu; Wang, Zhiming; Hu, Xianming
Tetrahedron Letters, 2012 , vol. 53, # 49 p. 6654 - 6656,3
反应条件
bismuth trifluoromethanesulphonate in acetonitrile
T=82°C; 8 h; regioselective reaction;
参考文献
Zhang, Xue-Lin; Wu, Qin-Pei; Zhang, Qing-Shan
Journal of Chemical Research, 2013 , vol. 37, # 11 p. 677 - 680
反应条件
hydrogenchloride; air in 1,4-dioxane; dimethyl sulfoxide
T=80°C; 6 h;
参考文献
Tanaka, Shin-Ya; Yasuda, Makoto; Baba, Akio
Journal of Organic Chemistry, 2006 , vol. 71, # 2 p. 800 - 803
反应条件
di-isopropylperoxydicarbonate in benzene
T=60°C; 4 h;
参考文献
Leardini, Rino; Nanni, Daniele; Tundo, Antonio; Zanardi, Giuseppe
Gazzetta Chimica Italiana, 1989 , vol. 119, # 12 p. 637 - 642
反应条件
methanol; chlorosulfonic acid
参考文献
Erdos
Angewandte Chemie, 1951 , vol. 63, p. 329
Full Text Show Details
Erdos; Gonzales
Ciencia, 1947 , vol. 8, p. 175
反应条件
1: 4 percent / InCl3 / acetonitrile / 0.05 h / Heating; microwave irradiation
View Scheme
参考文献
Duvelleroy, Dorothee; Perrio, Cecile; Parisel, Olivier; Lasne, Marie-Claire
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 20 p. 3794 - 3804
反应条件
1: 4 percent / InCl3 / acetonitrile / 0.05 h / Heating; microwave irradiation
View Scheme
参考文献
Duvelleroy, Dorothee; Perrio, Cecile; Parisel, Olivier; Lasne, Marie-Claire
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 20 p. 3794 - 3804
反应条件
indium(III) chloride in acetonitrile
aza-Diels-Alder reaction; 0.05 h; Heatingmicrowave irradiation;
参考文献
Duvelleroy, Dorothee; Perrio, Cecile; Parisel, Olivier; Lasne, Marie-Claire
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 20 p. 3794 - 3804
反应条件
indium(III) chloride in acetonitrile
aza-Diels-Alder reaction; 0.05 h; Heatingmicrowave irradiation; Title compound not separated from byproducts;
参考文献
Duvelleroy, Dorothee; Perrio, Cecile; Parisel, Olivier; Lasne, Marie-Claire
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 20 p. 3794 - 3804