1: 86 percent / BBr3 / CH2Cl2 / 16 h / -78 °C
2: 85 percent / Fremy's salt, KH2PO4 / H2O; acetone / 0.5 h / Ambient temperature
View Scheme
参考文献
Martin, Tracey; Moody, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 235 - 240
boron tribromide in dichloromethane
T=-78°C; 16 h;
参考文献
Martin, Tracey; Moody, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 235 - 240
