2-溴-3-氧代-4,4,4-三氟丁酸乙酯合成路线 （共 5 条）
反应条件
1: With anhydrous magnesium perchlorate T=0 - 5°C; 0.0833333 h; 2: With NBSacc T=0 - 5°C;
参考文献
Alinezhad, Heshmatollah; Tajbakhsh, Mahmood; Tehrani, Shahram Shahriari
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 5 p. 1543 - 1546
反应条件
1-n-butyl-3-methylimidazolium tetrafluoroborate T=20°C; 0.75 h; Ionic liquid;
参考文献
Meshram; Ramesh; Santosh Kumar; Chennakesava Reddy
Tetrahedron Letters, 2010 , vol. 51, # 33 p. 4313 - 4316
反应条件
in ethanol Ambient temperature1) rt, 4 h, 2) reflux, 3 h;
参考文献
Tanaka, Kiyoshi; Nomura, Kazuto; Oda, Hitoshi; Yoshida, Shouhei; Mitsuhashi, Keiryo
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 4 p. 907 - 911
反应条件
in ethanol 16 h; Ambient temperature;
参考文献
Journal of Heterocyclic Chemistry, , vol. 28, # 4 p. 907 - 911
反应条件
(i) aq. HBr, (ii) (heating); Multistep reaction;
参考文献
Cherbuliez,E. et al.
Helvetica Chimica Acta, 1965 , vol. 48, p. 1423 - 1426
