2-乙氧基-1,3-二氧戊环合成路线 (共 69 条)
反应条件
dibenzoyl peroxide T=79.9°C; var. temperatures; relation of the initial rate of formation to the concentration of the ortho ester; Product distributionMechanism;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 52, # 9 p. 2126 - 2132,1893 - 1898
反应条件
dibenzoyl peroxide T=100°C; 2 h; other temperature, other time; Rate constantProduct distribution;
参考文献
Rol'nik, L. Z.; Pastushenko, E. V.; Zlot-skii, S. S.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 10 p. 2363 - 2367,2131 - 2134
反应条件
toluene-4-sulfonic acid T=100°C; 5 h; other catalysts, variation of condition; Product distribution;
参考文献
Zhurkina, I. P.; Nedogrei, E. P.; Musavirov, R. S.; Kondrat'eva, I. A.; Rakhmankulov, D. L.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 12 p. 1338 - 1342
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , vol. 25, # 12 p. 1607 - 1611
反应条件
hydrogenchloride in toluene T=40°C; 8 h; Further byproducts given;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 55, # 8 p. 1786 - 1792,1586 - 1592
反应条件
T=16 - 20°C; 1 h; Further byproducts given;
参考文献
Zhurkina, I. P.; Nedogrei, E. P.; Musavirov, R. S.; Kondrat'eva, I. A.; Rakhmankulov, D. L.
J. Appl. Chem. USSR (Engl. Transl.), 1990 , vol. 63, # 2.2 p. 370 - 375,349 - 353
反应条件
sulfuric acid T=20°C; 1 h; Yield given;
参考文献
Zhurkina, I. P.; Nedogrei, E. P.; Musavirov, R. S.; Kondrat'eva, I. A.; Rakhmankulov, D. L.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 12 p. 1338 - 1342
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , vol. 25, # 12 p. 1607 - 1611
反应条件
toluene-4-sulfonic acid in tetrachloromethane T=20°C; reaction rate, activation energy;
参考文献
Nedogrei, E. P.; Zhurkina, I. P.; Musavirov, R. S.; Syrkin, A. M.; Rakhmankulov, D. L.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 5.2 p. 934 - 936
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 5 p. 1081 - 1083
参考文献
Zhurkina, I. P.; Nedogrei, E. P.; Musavirov, R. S.; Kondrat'eva, I. A.; Rakhmankulov, D. L.
J. Appl. Chem. USSR (Engl. Transl.), 1990 , vol. 63, # 2.2 p. 370 - 375,349 - 353
反应条件
nitric acid T=20°C; 24 h; var. catalysts, reaction times, educt ratios, temperatures, other dioxolane; Product distribution;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 60, # 11 p. 2491 - 2495,2227 - 2230
反应条件
toluene-4-sulfonic acid T=100°C; 5 h; other catalysts, variation of condition; Product distribution;
参考文献
Zhurkina, I. P.; Nedogrei, E. P.; Musavirov, R. S.; Kondrat'eva, I. A.; Rakhmankulov, D. L.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 12 p. 1338 - 1342
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , vol. 25, # 12 p. 1607 - 1611