反应条件
1: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / Inert atmosphere
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 160 °C / Inert atmosphere; Microwave irradiation
3: 5 Pd(II)/C(eggshell); hydrogen; palladium(II) oxide hydrate / tetrahydrofuran / 2 h / Inert atmosphere
View Scheme
参考文献
Van Oosten, Erik M.; Wilson, Alan A.; Mamo, David C.; Pollock, Bruce G.; Mulsant, Benoit H.; Houle, Sylvain; Vasdev, Neil
Canadian Journal of Chemistry, 2010 , vol. 88, # 12 p. 1222 - 1232