1-(3-三氟甲基苯基)乙醇合成路线 （共 40 条）
反应条件
phosphorus pentoxide in benzene 4 h; Heating;
参考文献
Mesnard, Danielle; Bernadou, Francoise; Miginiac, Leone
Journal of Chemical Research, Miniprint, 1981 , # 9 p. 3216 - 3245
反应条件
T=145 - 170°C; P=130 - 140 Torr;
参考文献
Bachman; Lewis
Journal of the American Chemical Society, 1947 , vol. 69, p. 2022
参考文献
Marvel et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 736
反应条件
pyridine; phosphorus tribromide in diethyl ether
参考文献
May and Baker Limited
Patent: US4185992 A1, 1980 ;
反应条件
1: KHSO4 2: (i) Br2, (ii) KOH 3: KOH View Scheme
参考文献
Mesnard, Danielle; Bernadou, Francoise; Miginiac, Leone
Journal of Chemical Research, Miniprint, 1981 , # 9 p. 3216 - 3245
反应条件
palladium diacetate; oxygen; (-)-sparteine in 1,2-dichloro-ethane T=60°C;
参考文献
Journal of the American Chemical Society, , vol. 123, # 30 p. 7475 - 7476
反应条件
1: With (-)-(R,R)-TADDOL; aluminum isopropoxide in diphenylether T=90°C; 1 h; 2: α-methyl-3-trifluoromethylbenzyl alcohol in diphenylether T=90°C; 0.166667 h; Product distribution / selectivity;
参考文献
US2009/30235 A1, ;
Page/Page column 12 ;
反应条件
[(C4Ph4COHOCC4Ph4)(μ-H)][(CO)4Ru2]; Novozym(R) 435; 2,4-dimethylpentan-3-one in toluene T=70°C; P=142.511 Torr; 40 h;
参考文献
Tetrahedron Asymmetry, , vol. 16, # 9 p. 1603 - 1610
反应条件
1: diisopropyl ether / 4 h / 30 °C / lipase QL 2: LiAlH4 / diethyl ether / 6 h / Heating View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 7, # 11 p. 3285 - 3294
反应条件
M. esculenta enzyme preparation immobilized on alginate gel in diethyl ether T=45°C; 116 h;
参考文献
Tetrahedron Asymmetry, , vol. 19, # 12 p. 1418 - 1423
