N-苯基-N-间硝基苯胺合成路线 （共 27 条）
反应条件
1: Raney nickel; ethanol 2: pyridine View Scheme
参考文献
Albert
Journal of the Chemical Society, 1948 , p. 1225,1230
反应条件
1: triethylamine / dichloromethane / 2 h / 0 - 20 °C 2: hydrogen / palladium 10 on activated carbon / dichloromethane; methanol View Scheme
参考文献
WO2012/59932 A1, ;
WO 2012/059932 A1
反应条件
triethylamine in dichloromethane T=0 - 20°C; 2 h;
参考文献
WO2012/59932 A1, ;
Page/Page column 125 ;
WO 2012/059932 A1
反应条件
copper-exchanged fluorapatite in methanol
T=20°C; 6 h;
参考文献
Kantam, M. Lakshmi; Venkanna, Gopaldasu T.; Sridhar, Chidara; Sreedhar, Bojja; Choudary, Boyapati M.
Journal of Organic Chemistry, 2006 , vol. 71, # 25 p. 9522 - 9524
反应条件
anhydrous iron chloride; caesium carbonate; copper(II) oxide; 1,1'-binaphthyl-2,2'-diol in N,N-dimethyl-formamide
T=80°C; 12 h; Inert atmosphere;
参考文献
Wang, Zhe; Fu, Hua; Jiang, Yuyang; Zhao, Yufen
Synlett, 2008 , # 16 p. 2540 - 2546
反应条件
potassium phosphate; copper(l) iodide in N,N-dimethyl-formamide
T=110°C; Ullmann condensation; 30 h;
参考文献
Rao, Honghua; Jin, Ying; Fu, Hua; Jiang, Yuyang; Zhao, Yufen
Chemistry - A European Journal, 2006 , vol. 12, # 13 p. 3636 - 3646
反应条件
potassium hydroxide; tris(dibenzylideneacetone)dipalladium (0); 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in water
T=60°C; 8 h;
参考文献
Huang, Xiaohua; Anderson, Kevin W.; Zim, Danilo; Jiang, Lei; Klapars, Artis; Buchwald, Stephen L.
Journal of the American Chemical Society, 2003 , vol. 125, # 22 p. 6653 - 6655
反应条件
copper diacetate; triethylamine
T=20°C; 24 h; Reagent/catalystSolventConcentrationTemperature;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Davan, Elham Etemadi; Rostami, Abed; Nematollahi, Arash
Journal of Organometallic Chemistry, 2013 , vol. 740, p. 123 - 130
反应条件
toluene-4-sulfonic acid
T=165°C; 0.833333 h; Ionic liquidMicrowave irradiation;
参考文献
Singh, Rahul; Allam, Bharat Kumar; Raghuvanshi, Dushyant Singh; Singh, Krishna Nand
Tetrahedron, 2013 , vol. 69, # 3 p. 1038 - 1042
反应条件
in dichloromethane
T=20°C; 6 h; Molecular sieve;
参考文献
Luo, Jun; Ji, Enwei; Ye, Jingyuan; Wu, Runze; Qiu, Lei
Tetrahedron Letters, 2013 , vol. 54, # 34 p. 4505 - 4508
