4,4-二苯基-2-环己烯-1-酮合成路线 (共 22 条)
反应条件
tert.-butylhydroperoxide; dipyridinium dichromate; Celite in tert-butyl alcohol; benzene T=20°C; 26 h;
参考文献
Zimmerman, Howard E.; Nesterov, Evgueni E.
Journal of the American Chemical Society, 2002 , vol. 124, # 11 p. 2818 - 2830
反应条件
potassium hydroxide in ethanol Condensation;
参考文献
Senthil Kumar; Nangia, Ashwini
Acta Crystallographica Section C: Crystal Structure Communications, 2000 , vol. 56, # 3 p. 360 - 361
反应条件
lithium aluminium tetrahydride in tetrahydrofuran; diethyl ether 0.5 h; Heating;
参考文献
Zimmerman, Howard E.; Pasteris, Robert J.
Journal of Organic Chemistry, 1980 , vol. 45, # 24 p. 4876 - 4891
反应条件
1: 98 percent / t-BuOK / various solvent(s) / 20 °C 2: PTSA / toluene 3: Red-Al / toluene / 0 - 20 °C View Scheme
参考文献
Zimmerman, Howard E.; Pasteris, Robert J.
Journal of Organic Chemistry, 1980 , vol. 45, # 24 p. 4876 - 4891
反应条件
1: PTSA / toluene 2: Red-Al / toluene / 0 - 20 °C View Scheme
参考文献
Zimmerman, Howard E.; Pasteris, Robert J.
Journal of Organic Chemistry, 1980 , vol. 45, # 24 p. 4876 - 4891
反应条件
dipyridine chromium trioxide in dichloromethane
参考文献
Dauben,W.G. et al.
Journal of Organic Chemistry, 1969 , vol. 34, # 11 p. 3587 - 3592
反应条件
1: 89.0 percent Chromat. / H2SO4 / acetic acid / 1.5 h / 104 °C / other acid catalysts 2: KOH / ethanol / 2.78 h / -5 - 6 °C View Scheme
参考文献
Amedio Jr., John C.; Bernard, Paul J.; Fountain, Mark; Van Wagenen Jr., Gerritt
Synthetic Communications, 1998 , vol. 28, # 20 p. 3895 - 3906
反应条件
1: 95 percent / m-CPBA / CH2Cl2 / 30 h / 0 °C 2: 80 percent / BF3*OEt2 / CH2Cl2 / 0.5 h / 0 °C 3: 50 percent / KOH / ethanol; tetrahydrofuran / 4 h / 0 - 20 °C View Scheme
参考文献
Roy, Saikat; Banerjee, Rahul; Nangia, Ashwini; Kruger, Gert J.
Chemistry - A European Journal, 2006 , vol. 12, # 14 p. 3777 - 3788
反应条件
1: 80 percent / BF3*OEt2 / CH2Cl2 / 0.5 h / 0 °C 2: 50 percent / KOH / ethanol; tetrahydrofuran / 4 h / 0 - 20 °C View Scheme
参考文献
Roy, Saikat; Banerjee, Rahul; Nangia, Ashwini; Kruger, Gert J.
Chemistry - A European Journal, 2006 , vol. 12, # 14 p. 3777 - 3788
反应条件
sodium hydroxide; ozone 1.) CH2Cl2, MeOH, -78 deg C, 2.) MeOH; Yield given. Multistep reaction;
参考文献
DeNinno, Michael P.; McCarthy, Keith E.
Tetrahedron, 1997 , vol. 53, # 32 p. 11007 - 11020